4.7 Article

P,C-bond cleavage in the ligand sphere of a nickel(II) complex

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DALTON TRANSACTIONS
卷 44, 期 3, 页码 1317-1322

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ROYAL SOC CHEMISTRY
DOI: 10.1039/c4dt02158d

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  1. DFG-funded transregional collaborative research centre Cooperative effects in homo- and heterometallic complexes (3MET) [SFB/TRR 88]

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Reacting nickel(II) perchlorate with a bidentate P,N-ligand in methanol leads to P,C-bond cleavage and gives a five-coordinate nickel complex wherein the nickel(II) site is coordinated by a tridentate P,N,P-ligand and a bidentate N,C-ligand. The carbanion of the latter is the result of the P,C-bond cleaving process. The diamagnetic nickel(II) complex was characterized by means of elemental analysis, NMR spectroscopy, cyclic voltammetry and X-ray structure analysis.

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