期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 18, 期 22, 页码 4164-4168出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0ob00697a
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资金
- DST-SERB, India [EMR/2016/004040]
- UGC-New Delhi
A direct and metal free one-pot method has been developed for the stereoselective synthesis of tetrahydropyrimidinone derivatives from a vinyl arene and formaldehyde using a tartaric acid-dimethylurea (TA : DMU) melt as a green reaction medium. The substrate scope of this method is very general and the tetrahydropyrimidinone (THPM) derivatives are synthesized in good yields with a high degree of diastereoselectivity. In this reaction, the melt plays a triple role as the solvent, catalyst and reagent.
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