期刊
GREEN CHEMISTRY
卷 22, 期 12, 页码 3952-3955出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0gc00865f
关键词
-
资金
- National Natural Science Foundation of China [21801142]
- Ningbo Municipal Natural Science Foundation [2019A610021]
A concise and eco-friendly acylation/cyclization of 1,6-dienes with linear ethers under catalyst- and base-free conditions has been developed.tert-Butyl hydroperoxide (TBHP)-promoted tandem cleavage of C(sp(3))-H and C(sp(3))-O bonds of linear ethers is the key in this process, which provides a straightforward and efficient method to realize acylation reaction. The significant advantages of this method include catalyst- and base-free, mild reaction conditions, high scalability, operational simplicity, ease of scale-up, dual roles of ethers and controllable synthesis.
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