期刊
RSC ADVANCES
卷 10, 期 55, 页码 33155-33160出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0ra07212e
关键词
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资金
- Department of Education of Guangdong Province [2018KQNCX236, 2019KTSCX162]
- Science and Technology Project of Guangdong Province [408-99000213]
- Science and Technology Project of Shaoguang city [2018sn047, 2019sn055]
- Shaoguan University [408-9900416, 408-99000618]
- National undergraduate innovation and entrepreneurship project [201810576016]
- National Natural Science Foundation of China [21961002]
- Gannan Medical University [YJ202027]
An efficient electrochemical transformation of a variety of alkenes and sulfonyl hydrazides into vinyl sulfones with a catalytic amount of tetrabutylammonium iodide in water is reported. The reaction proceeds smoothly to afford vinyl sulfones with good selectivities and yields at room temperature under air in an undivided cell. Cyclic voltammograms and control experiments have been performed to provide preliminary insight into the reaction mechanism. The key features of this reaction include using pure water as solvent, transition metal- and oxidant-free conditions, and being easily scaled up to gram-scale synthesis.
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