期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 18, 期 38, 页码 7545-7548出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0ob01815e
关键词
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Lewis acid-assisted palladium-catalysed dealkoxylation ofN-alkoxyamides has been developed. This reaction proceeded smoothly with a range ofN-alkoxyamides in the absence of an external reductant, thereby establishing a convenient and reductant-free protocol. In addition, a gram-scale reaction could be achieved. Preliminary mechanistic investigations indicated that beta-hydrogen elimination from a palladium alkoxide intermediate generated an intramolecular hydride source.
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