期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 85, 期 23, 页码 15622-15630出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.0c02459
关键词
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资金
- Fundacao de Amparo a Pesquisa do Estado de Minas Gerais (FAPEMIG)
- Conselho Nacional de Desenvolvimento Cientifico e Tecnologico (CNPq)
- Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior-Brasil (CAPES) [001, 0673/13-CT-Infra-FINEP, 09/2016]
- Programa de Pesquisa e Aplicada-Fundacao Araucaria de Apoio ao Desenvolvimento Cientifico e Tecnologico do Estado do Parana
- CNPq
- National Program for Academic Cooperation (PROCAD) of CAPES/Brazil
The use of star anise oil from a natural source as a dienophile in the multicomponent double Povarov reaction (MCPRs) to produce highly substituted julolidines with diverse technological applications is described. Within the framework of green chemistry, these MCPRs have many advantages such as (i) use of water in the reaction, (ii) creation of up to six bonds in one sequence, (iii) water as a sole waste, (iv) 100% of carbon economy, (v) a metal-free process, and (vi) nontoxic and reusable organocatalysts. These advantages, along with a simple workup procedure, make this protocol greener for the synthesis of julolidines.
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