期刊
GREEN CHEMISTRY
卷 19, 期 11, 页码 2510-2514出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7gc01103b
关键词
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资金
- Universita degli Studi di Perugia
- MIUR [PGR123GHQY]
Herein we report the unprecedented Fujiwara-Moritani reaction catalysed by the commercially available heterogeneous palladium catalyst Pd/C. The reaction works efficiently in GVL, a biomass derived solvent, in the coupling between variously substituted acetanilides and electron-poor alkenes, with complete selectivity towards the ortho-substitution. Moreover, the catalyst can be easily recycled and reused for consecutive reaction runs. We also developed a continuous-flow procedure, through an easily accessible tailor-made reactor, which allows the production of C-H alkenylated products on grams per hour scale.
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