期刊
GREEN CHEMISTRY
卷 19, 期 11, 页码 2541-2545出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7gc00909g
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资金
- Sigma-Aldrich Chemicals Pvt. Ltd, Bangalore
Herein, we report the metal free and intramolecular hydrogen bonding (IMHB) directed (Z)-selective synthesis of amide substituted beta-aminoenones. Systematically, we confirm the role of dual IMHB (C=O center dot center dot center dot H-N) on the Z-direction using single-crystal X-ray analysis and 1D and 2D NMR studies. High stereoselectivity, atom efficiency, excellent yields and high purity are achieved by mere filtration. We avoid column purification and the formed by-product in the process is environmentally friendly.
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