期刊
FOOD CHEMISTRY
卷 221, 期 -, 页码 1298-1307出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.foodchem.2016.11.026
关键词
Honey; Royal jelly; Multiclass residue; QuEChERS; HPLC-MS/MS; Veterinary drug
资金
- National Natural Science Foundation of China [31201859]
- National Project of Risk Assessment for Quality and Safety of Special Agro-products
- National Key Project for Agro-product Quality & Safety Risk Assessment, PRC [GJFP2015010]
- Agricultural Science and Technology Innovation Program [CAAS-ASTIP-2015-IAR]
The aim of this study was to develop an analytical method for the analysis of a wide range of veterinary drugs in honey and royal jelly. A modified sample preparation procedure based on the quick, easy, cheap, effective, rugged and safe (QuEChERS) method was developed, followed by liquid chromatography tandem mass spectrometry determination. Use of the single sample preparation method for analysis of 42 veterinary drugs becomes more valuable because honey and royal jelly belong to completely different complex matrices. Another main advantage of the proposed method is its ability to identify and quantify 42 veterinary drugs with higher sensitivity than reference methods of China. This work has shown that the reported method was demonstrated to be convenient and reliable for the quick monitoring of veterinary drugs in honey and royal jelly samples. (C) 2016 Elsevier Ltd. All rights reserved.
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