期刊
FOOD CHEMISTRY
卷 217, 期 -, 页码 191-195出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.foodchem.2016.08.101
关键词
Acrylamide; QuEChERS; LC-ESI-MS-Triple Quadrupole; Dried fruits; Dried prunes; Peanuts
Acrylamide is a carcinogenic and neurotoxic process contaminant that is generated from food components during heat treatment, while it is absent in raw foodstuffs. Its level in food arouses great concern. A method for acrylamide extraction and determination in dried fruits (dried prunes and raisins) and edible seeds (almonds, hazelnuts, peanuts, pine nuts, pistachios, and walnuts) using a QuEChERS-LC-ESI-MS-Triple Quadrupole approach was set up. Linearity, sensitivity, accuracy, and precision of the method were satisfactory. Dried prunes and peanuts were the only samples appreciably contaminated, 14.7-124.3 and 10.0-42.9 mu g/kg, respectively, as a consequence of the drying process. In fact, prunes are dried at 70-80 degrees C for a quite long time (24-36 h), while peanuts undergo a roasting process at 160-180 degrees C for 25-30 min. The relative standard deviations, accuracy, LOD, and LOQ show that the method provides a reliable approach to acrylamide determination in different matrices. (C) 2016 Elsevier Ltd. All rights reserved.
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