期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 19, 期 19, 页码 4327-4337出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/d1ob00300c
关键词
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资金
- Strategic Priority Research Program of the Chinese Academy of Sciences [XDB20000000]
- CAS [QYZDY-SSW-SLH029]
- NSFC [21725205, 21572246, 22001112, 21702223, 2207126]
- Key-Area Research and Development Program of Guangdong Province [2020B010188003]
- [STCSM-18520712200]
A series of unsaturated carbonyls, quinones, and pyridinium salts have been successfully reduced to the corresponding saturated carbonyls, dihydroxybenzenes, and hydropyridines in moderate to high yields using tetrahydroxydiboron/water as a mild, convenient, and metal-free reduction system. Deuterium-labeling experiments have shown this protocol to be an exclusive transfer hydrogenation process from water.
A series of unsaturated carbonyls, quinones, and pyridinium salts have been effectively reduced to the corresponding saturated carbonyls, dihydroxybenzenes, and hydropyridines in moderate to high yields with tetrahydroxydiboron/water as a mild, convenient, and metal-free reduction system. Deuterium-labeling experiments have revealed this protocol to be an exclusive transfer hydrogenation process from water.
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