4.7 Article

A photochemical ring expansion of 6-to 8-membered nitrogen heterocycles by [1,3]-sigmatropic rearrangement

期刊

CHEMICAL COMMUNICATIONS
卷 57, 期 37, 页码 4556-4559

出版社

ROYAL SOC CHEMISTRY
DOI: 10.1039/d1cc00393c

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资金

  1. European Regional Development Fund [ERDF Interreg Va programme] [121]
  2. EPSRC [EP/P013341/1, EP/L003325/1, EP/K039466/1]
  3. EPSRC [EP/L003325/1, EP/P013341/1, EP/K039466/1] Funding Source: UKRI

向作者/读者索取更多资源

A new route to azocines and benzoazocines from furopyridinones is described through a photochemically induced [1,3]-sigmatropic rearrangement. The method provides excellent atom economy by sequencing thermal and photochemical ring expansion steps under continuous flow.
A new route to azocines and benzoazocines from furopyridinones is described through a photochemically induced [1,3]-sigmatropic rearrangement. The method gives access to these 8-membered nitrogen heterocycles from dimethyl squarate in four stages and with excellent atom economy by sequencing thermal and photochemical ring expansion steps under continuous flow.

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