期刊
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
卷 2017, 期 32, 页码 4740-4748出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201700744
关键词
Iodine; Chalcogens; Green chemistry; Solvent free; Microwave; Synthetic methods; Iodine-mediated reactions
资金
- GlaxoSmithKline (GSK)
- Sao Paulo Research Foundation (FAPESP) [2014/50249-8]
- Instituto Nacional de Ciencia e Tecnologia (INCT)-Catalise
- Fundacao de Amparo a Pesquisa e Inovacao do Estado de Santa Catarina (FAPESC)-Pronex [HEC-SRGP-161]
- Financiadora de Estudos e Projetos (FINEP)
- CNPq
We have developed a green and efficient protocol for the chalcogenation of bicyclic arenes by using I-2/DMSO as catalytic system under solvent- and metal-free conditions. This protocol allows access to several chalcogenated bicyclic arenes through C(sp(2))-H bond functionalization, in good to excellent yields by using microwave irradiation or conventional heating.
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