☆ 4.7 Review

Photomechanical crystalline materials: new developments, property tuning and applications

CRYSTENGCOMM (2022)

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Summary: The rational combination of suitable functionalities in single crystalline materials has led to the development of multistimuli-receptive actuators. The one-dimensional coordination polymer fabricated in this study displays all dynamic effects of photo-, thermo-, and mechano-responsiveness, paving the way for designing multisalient actuating materials.

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Article Chemistry, Multidisciplinary

Cocrystal Engineering: Toward Solution-Processed Near-Infrared 2D Organic Cocrystals for Broadband Photodetection

Yu Wang et al.

Summary: Large-area 2D cocrystals with strong near-infrared absorption have been successfully designed and prepared through intermolecular charge-transfer interactions. Tuning the growth solvents and processes allows for morphological control, resulting in enhanced CT absorption and excellent device performance in the NIR region. Transient absorption spectroscopy and device configuration optimization play key roles in generating long-lived free charge carriers and improving the responsivity and response time of the cocrystals.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2021)

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Article Chemistry, Multidisciplinary

Light-Powered Autonomous Flagella-Like Motion of Molecular Crystal Microwires

Fei Tong et al.

Summary: This study demonstrates that (Z)-DVAM molecular crystalline microwires can exhibit continuous oscillatory motion when exposed to a combination of ultraviolet and visible light, mimicking the behavior of biological flagella. This is the first example of molecular crystals showing complex oscillatory behavior under continuous irradiation, with rotational frequency depending on light intensity and polarization.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2021)

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Article Chemistry, Applied

Spatial photocontrol of the passive optical output direction of the elastic molecular crystals based on acylhydrazone derivatives

Jiang Peng et al.

Summary: The study investigates the reversible E-Z isomerization reactions and photomechanical behaviors of photo-reactive acylhydrazone derivatives in crystals. Different shaped crystals exhibit varying properties under light exposure, suggesting potential applications in crystal actuators and position-controllable optical transducers.

DYES AND PIGMENTS (2021)

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Review Chemistry, Multidisciplinary

Mechanically Responsive Organic Crystals by Light

Hideko Koshima et al.

Summary: Recent studies have focused on mechanically responsive molecular crystals that exhibit macroscopic motions through light and heat, with potential applications in sensors, switches, actuators, and soft robots.

ISRAEL JOURNAL OF CHEMISTRY (2021)

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Review Materials Science, Multidisciplinary

Recent Advances on Molecular Crystalline Luminescent Materials for Optical Waveguides

Siqin Wu et al.

Summary: Molecule-based fluorescent materials with optical waveguides (MFOWs) have unique photoluminescence properties and cover the entire visible light region. Research progress on MFOWs and emerging materials for high-performance applications are summarized, offering potential guidance for future design and development of MFOWs.

ADVANCED OPTICAL MATERIALS (2021)

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Article Chemistry, Physical

Structural Origins of Elastic and 2D Plastic Flexibility of Molecular Crystals Investigated with Two Polymorphs of Conformationally Rigid Coumarin

Keke Zhang et al.

Summary: This study investigates the mechanical behaviors of two polymorphs of the structurally rigid molecule coumarin, revealing that form I crystals exhibit high elasticity while form II crystals are 2D plastic and twistable. The differences in mechanical behaviors are attributed to the molecular packing and interactions of coumarin rather than molecular flexibility.

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Susan A. Bourne

IUCRJ (2021)

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Light-Driven Rapid Peeling of Photochromic Diarylethene Single Crystals

Masato Tamaoki et al.

Summary: The article discusses a rapidly photoresponsive behavior exhibited by photochromic diarylethene crystals, including peeling, jumping, and cracking, under different photoirradiation conditions. The study explores the details of the rapid photoresponsive peeling based on molecular packings and the crystal size. These crystals show potential applications as macroscopic photomechanical actuators driven by molecular machinery.

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(9-Isocyanoanthracene)gold(I) Complexes Exhibiting Two Modes of Crystal Jumps by Different Structure Change Mechanisms

Kenta Kato et al.

Summary: The first examples of single crystals exhibiting salient effects by different structure change mechanisms are reported, including photodimerization reaction-induced photosalient effect and anisotropic thermal contraction-induced thermosalient effect. Multiple jumps of crystals by cooling and then UV irradiation are demonstrated for the programmed motion of molecular crystals.

INORGANIC CHEMISTRY (2021)

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JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2021)

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Rapidly Reversible Organic Crystalline Switch for Conversion of Heat into Mechanical Energy

Madushani Dharmarwardana et al.

Summary: Solid-state thermoelastic behavior is rare in organic crystals, but a fully reversible thermomorphic actuator has been developed that can operate for multiple years and perform over 200 cycles of actuation with rapid, predictable directional force.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2021)

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Article Chemistry, Multidisciplinary

Stepwise introduction of three different transition metals in metallo-supramolecular polymer for quad-color electrochromism

Manas Kumar Bera et al.

Summary: The stepwise introduction of three different transition metals into a metallo-supramolecular polymer has successfully led to the synthesis of a polymer with quad-color electrochromic properties. This synthetic method can be extended to fabricate other MSPs with different compositions, exhibiting a broad optical and electrochemical window.

COMMUNICATIONS CHEMISTRY (2021)

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Article Chemistry, Physical

Mechanical Bending and Modulation of Photoactuation Properties in a One-Dimensional Pb(II) Coordination Polymer

Bibhuti Bhusan Rath et al.

Summary: As research on stimuli-responsive materials progresses, dynamic crystals are leading the investigation, while studies on the mechanical properties of coordination polymers (CPs) are still in their infancy. The report of one-dimensional CP with unique properties provides a new avenue for designing CPs with multi-stimuli-responsive actuating properties.

CHEMISTRY OF MATERIALS (2021)

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Article Chemistry, Multidisciplinary

Cocrystallization Enabling Photoinduced Rotation of an Azopyridine Crystal

Rongli Wei et al.

Summary: A novel 2:1 cocrystal of APO3C and TFTA was designed and synthesized in this study, which achieved photoinduced rotation with the three indispensable factors of the linear synthon induced by hydrogen bonding, unsymmetrical isomerization of APO3C molecules, and their diagonal arrangement.

CRYSTAL GROWTH & DESIGN (2021)

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Article Chemistry, Multidisciplinary

Photothermally Driven High-Speed Crystal Actuation and Its Simulation

Shodai Hasebe et al.

Summary: This study reports on photothermally driven fast-bending actuation of a crystal, with successful simulation of the driving process. Thick crystals can bend quickly, while thin crystals bend due to photoisomerization. High-frequency bending is also achievable through the photothermal effect.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2021)

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Article Chemistry, Multidisciplinary

Preparation and solid-state characterization of dapsone pharmaceutical cocrystals through the supramolecular synthon strategy

Chenyang Zhao et al.

Summary: This paper investigates the new solid forms of Dapsone using crystal engineering method of cocrystallization, specifically focusing on the formation of DAP-PYR cocrystals with the aid of supramolecular synthon -NH2μpyridine. The experimental results indicate that the formation of DAP-PYR cocrystals mainly depends on the initial feed ratio of raw materials, and hydrogen bonding plays a crucial role in promoting the formation of these cocrystals.

CRYSTENGCOMM (2021)

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Article Chemistry, Multidisciplinary

Anisotropic bending and twisting behaviour of a twin crystal composed of a diarylethene

Takuya Higashiguchi et al.

Summary: The crystals formed by 1,2-bis(2-methyl-5-(4-undecyloxyphenyl)-3-thienyl)-perfluorocyclopentene demonstrated unique photomechanical bending behavior under UV light irradiation, with bending velocity depending on lighting directions. This crystal was identified as a twin crystal through X-ray crystallography, and the bending mechanism was found to be influenced by twin components, absorption anisotropy of diarylethene molecules, and crystal twisting degree.

CRYSTENGCOMM (2021)

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Actuation performance of a photo-bending crystal modeled by machine learning-based regression

Kazuki Ishizaki et al.

Summary: This study introduces a machine learning-based regression approach for modeling the deflection and force of a photo-bending crystal. Results show that by analyzing experimental measurements and feature values, the most fitted models can be constructed to explain material mechanics-related properties.

CRYSTENGCOMM (2021)

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Review Chemistry, Multidisciplinary

Dynamic effects in crystalline coordination polymers

Bibhuti Bhusan Rath et al.

Summary: CPs have emerged as relatively new crystalline materials with great potential in the field of mechanical properties, showing promise as leading candidates for multifunctional actuating materials.

CRYSTENGCOMM (2021)

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Article Chemistry, Multidisciplinary

Photomechanical response of sulfonylhydrazone molecular crystals

Pragyan J. Hazarika et al.

Summary: Sulfonylhydrazones are a novel type of organic molecular photoswitches. Four derivatives were examined for their photoresponse in solution and crystalline states, with SH-3 displaying the most significant photomechanical effect while SH-2 showed no photomechanical response.

CRYSTENGCOMM (2021)

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Article Materials Science, Multidisciplinary

Azobenzene crystal polymorphism enables tunable photoinduced deformations, mechanical behaviors and photoluminescence properties

Yunhui Hao et al.

Summary: This study reports the fabrication and preparation of polymorphic molecular crystals with multiple stimuli-responsive properties and multiple functionalities. Different polymorphic forms of the crystals exhibit diversity in photoinduced, mechanical and photoluminescence properties, providing a potential strategy for the development of smart materials.

JOURNAL OF MATERIALS CHEMISTRY C (2021)

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Article Chemistry, Multidisciplinary

Light-fueled rapid macroscopic motion of a green fluorescent organic crystal

Prasenjit Giri et al.

Summary: The new green fluorescent organic crystal displays various macroscopic responses under UV light, with shape deformation and actuation controlled by specific parts of the crystal and the direction of illumination. Experimental evidence suggests that the light-fueled macroscopic actuation of the E-ArF2 crystal is rooted in the combined effect of E-to-Z isomerization and [2 + 2] cycloaddition reaction in the solid state. A general mechanistic model of the actuation is proposed based on the experimental findings.

CRYSTENGCOMM (2021)

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Article Chemistry, Multidisciplinary

Photoinduced topographical surface changes and photoresponse of the crystals of 7-methoxycoumarin

Kanae Yano et al.

Summary: Photoinduced topographical changes were observed on the surface of a single crystal of 7-methoxycoumarin upon UV light irradiation, with different reactions and crystal formations depending on the wavelength of UV light. Additionally, photoinduced amorphization was found on the coumarin crystal surface, along with reverse bending after prolonged irradiation.

CRYSTENGCOMM (2021)

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Review Chemistry, Multidisciplinary

Functional flexible molecular crystals: intrinsic and mechanoresponsive properties

Tomohiro Seki et al.

Summary: Recent interest in functional flexible molecular crystals has the potential to provide unique optoelectronic applications and stimuli-responsive chemistry. The flexible behavior of molecular crystals, such as stress-induced response shape deformation, is another new feature realized by molecular and crystal structure design strategies. These molecular crystals with mechano-responsive properties have potential powerful applications, such as in wearable devices.

CRYSTENGCOMM (2021)

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Fluorine as a robust balancer for tuning the reactivity of topo-photoreactions of chalcones and the photomechanical effects of molecular crystals

Yuanhong Shu et al.

Summary: By synthesizing fluorine-free chalcones and chalcones with varying numbers of fluorine atoms, researchers found that the reactivity of photo-induced [2 + 2] cycloaddition reactions in crystals could be tuned by fluorine. The introduction of fluorine increased molecular planarity and strategically positioned reactive double bonds in crystal lattices. This led to stereospecific [2 + 2] cycloaddition reactions, resulting in various photomechanical behaviors in chalcone-based molecular crystals. The more efficient photo-induced reactions in crystalline states caused significant motions of the molecular crystals, demonstrating the potential of crystal engineering for fabricating mechanically responsive crystalline materials.

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Kevin R. Chalek et al.

Summary: The study demonstrates how a novel combination of techniques including ensemble oriented-crystal solid-state NMR, X-ray diffraction, and first principles computational modeling can establish the atomic-resolution mechanism for the photomechanical response of crystals composed of photoreactive molecules. The model constructed based on these techniques accurately predicts the elongation of the crystal nanorods. Understanding how molecular-level photochemistry generates mechanical displacements allows for the tuning of the expansion of the nanorods by controlling the initial orientation of the unit cell, offering new insights into the relationship between atomic-level structural rearrangement and mechanical response in nanostructured samples.

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Optical Waveguiding Organic Single Crystals Exhibiting Physical and Chemical Bending Features

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ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2020)

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