期刊
GREEN CHEMISTRY
卷 24, 期 12, 页码 4794-4799出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/d2gc00649a
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资金
- Department of Science and Technology (DST), New Delhi
- CSIR-IICT
This paper presents an approach for chemical synthesis using solar energy, utilizing an integrated programmed solar panel micro-flow platform for Wolff rearrangements to synthesize various compounds. The method does not require a metal catalyst and utilizes sunlight as an energy source, providing a greener and more efficient approach.
Employing solar energy for chemical synthesis is one of the most important reaction pathways on the earth. An integrated programmed solar panel micro-flow platform approach is presented herein for Wolff rearrangements to synthesize beta-amino acid, ester, amide, thiolate, etc. The reaction is performed without a metal catalyst and uses sunlight as an energy source in a time and labour-efficient manner leading to a greener approach. The synthesized homologated acid was further extended to the synthesis of an anti-diabetic type-2 active pharmaceutical ingredient (API), prositagliptin.
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