4.7 Article

Ruthenium(ii)-catalyzed synthesis of CF3-isoquinolinones via C-H activation/annulation of benzoic acids and CF3-imidoyl sulfoxonium ylides

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ORGANIC CHEMISTRY FRONTIERS
卷 9, 期 16, 页码 4388-4393

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ROYAL SOC CHEMISTRY
DOI: 10.1039/d2qo00839d

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  1. NSF of China [22071068]

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The ruthenium(ii)-catalyzed C-H activation/annulation reaction of benzoic acids and CF3-imidoyl sulfoxonium ylides, enabled by weak O-coordination, has been achieved to synthesize a series of 3-trifluoromethylisoquinolinones in yields ranging from 37% to 75%.
A ruthenium(ii)-catalyzed C-H activation/annulation reaction of benzoic acids and CF3-imidoyl sulfoxonium ylides enabled by weak O-coordination has been achieved. A series of 3-trifluoromethylisoquinolinones were synthesized in 37-75% yields under redox-neutral reaction conditions.

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