期刊
CHEMICAL COMMUNICATIONS
卷 58, 期 60, 页码 8344-8347出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/d2cc02344j
关键词
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资金
- JSPS KAKENHI [JP15H05849, JP17K06910, JP19K22186, JP20KK0121, JP21H01936, JP21H05080]
- AMED [JP20ak0101090, JP21ak0101156]
- CREST [JPMJCR18R1]
- JST A-step program [18067420]
- New Energy and Industrial Technology Development Organization (NEDO)
- Japan Keirin Autorace Foundation
- Ogasawara Foundation
This study demonstrates the rapid synthesis of unstable compounds using a fast electrochemical reactor, enabling easy access to various chemical reactions.
Flash (extremely fast) electrochemical generation of unstable arylbis(arylthio)sulfonium triflates [ArS(ArSSAr)](+) [OTf](-) that are unsuitable for accumulation in batch processes was achieved within 10 s in a divided-type flow electrochemcial reactor, enabling one-flow access to vinyl triflates, short-lived oxocarbenium triflates and glycosyl triflates.
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