期刊
INORGANIC CHEMISTRY FRONTIERS
卷 3, 期 8, 页码 1058-1064出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6qi00115g
关键词
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资金
- National Natural Science Foundation of China [21571154]
- Jiangsu Overseas Research & Training Program for University Prominent Young & Middle-aged Teachers and Presidents
- Leverhulme Trust [ECF-2013-414]
- ERC [247450]
- EPSRC [EP/F034210/1]
- Science City (AWM/ERDF)
The synthesis of nanoparticles of conjugates of caffeic acid-modified chitosan with ruthenium arene complexes is described. The chemical structure and physical properties of the nanoparticles were characterised by electronic absorption spectroscopy (UV-vis), Fourier transform infrared spectroscopy (FT-IR), H-1 NMR spectroscopy, dynamic light scattering (DLS), transmission electron microscopy (TEM), X-ray powder diffraction (XRD), and circular dichroism (CD) analysis. The multi-spectral results revealed that caffeic acid is covalently bound to chitosan and chelates to {Ru(p-cymene)Cl}(+). The DLS studies indicated that the Ru-caffeic acid modified chitosan nanoparticles are well-defined and of nanometre size. Such well-defined nanocomposites of chitosan and metal complexes might find a range of applications, for example in drug delivery.
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