期刊
CRYSTENGCOMM
卷 24, 期 38, 页码 6747-6750出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/d2ce00803c
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资金
- Deutsche Forschungsgemeinschaft (DFG, German Research Foundation) [387284271 - SFB 1349]
This study provides the first in situ real-time monitoring of the mechanochemical formation mechanism of mixed-ligand MOFs and reveals that binary phases can serve as intermediates or competing products in one-pot and stepwise synthesis.
The mechanism of mixed-ligand metal-organic framework (MOF) formation, and the possible role of intermediate single-ligand metal complexes during mechanosynthesis, have not been explored yet. For the first time, we report here in situ real-time monitoring of the mechanochemical formation mechanism of mixed-ligand MOFs. Our results show that binary phases can act as intermediates or competing products in one-pot and stepwise synthesis.
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