期刊
CHEMISTRYMETHODS
卷 2, 期 1, 页码 -出版社
WILEY
DOI: 10.1002/cmtd.202100068
关键词
mass spectrometry; on-line monitoring; pressurized sample infusion; reaction mechanisms; real-time monitoring
资金
- NSERC Discovery program
Pressurized sample infusion is a simple and effective method for continuously introducing a solution to a mass spectrometry source, allowing real-time data acquisition. It is applicable for various reactions that require real-time information.
Pressurized sample infusion (PSI) is a simple and effective means of continuously introducing a solution to an electrospray ionization mass spectrometry (ESI-MS) source. It allows for acquisition of real-time data in an air- and moisture-free environment and requires minimal additional infrastructure. It is applicable for use for any reaction in which one or more components are detectable by ESI-MS and for which time-course information is desired over a time scale of seconds to minutes. The strengths and weaknesses of the method are critically examined, and technique tips and tricks are provided to enable maximal effectiveness when employing this approach to continuous monitoring of complex reaction mixtures.
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