☆ 4.5 Review

A review of the use of Mxenes as hosts in lithium metal anodes and the anode formation

NEW CARBON MATERIALS (2023)

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Review Nanoscience & Nanotechnology

A Review of In-Situ Techniques for Probing Active Sites and Mechanisms of Electrocatalytic Oxygen Reduction Reactions

Jinyu Zhao et al.

Summary: Electrocatalytic oxygen reduction reaction (ORR) is crucial for electrochemical energy technologies. However, the identification of ORR active sites and the elucidation of ORR mechanisms are challenging due to the complex dynamic evolution of catalysts and intermediates. In-situ characterization techniques are necessary for real-time monitoring of catalyst structure, intermediate behavior, and product evolution. This review highlights the advances in using various in-situ techniques to study catalytic processes, including catalyst structure evolutions, intermediate adsorption/desorption behavior, and product nucleation and reconstruction. Challenges and prospects of in-situ techniques for future catalysts research in the ORR process are also discussed.

NANO-MICRO LETTERS (2023)

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Article Chemistry, Multidisciplinary

A BF3-Doped MXene Dual-Layer Interphase for a Reliable Lithium-Metal Anode

Mingwei Shang et al.

Summary: A dual-layer interphase consisting of an in-situ-formed lithium carboxylate organic layer and a thin BF3-doped monolayer Ti3C2 MXene on Li metal is reported. The honeycomb-structured organic layer increases the wetting of electrolyte, leading to a thin solid electrolyte interface (SEI). The BF3-doped monolayer MXene provides abundant active sites for lithium nucleation and growth, reducing the thickness of inorganic-rich components in the SEI layer.

ADVANCED MATERIALS (2023)

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Article Engineering, Environmental

Structure and performance insights in carbon dots-functionalized MXene-epoxy ultrathin anticorrosion coatings

Jiheng Ding et al.

Summary: Functionalized MXene nanosheets with carbon dots significantly improve the chemical stability of MXene in water and enhance the anticorrosion performance of epoxy composite coatings through a flow-induced approach. The unique structure of CD-Ti3C2Tx platelets inhibits corrosion-promotion activity and improves the stability and durability of the coatings for heavy-anticorrosion applications in harsh sea environments.

CHEMICAL ENGINEERING JOURNAL (2022)

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Article Materials Science, Multidisciplinary

Microstructure controlle d synthesis of Ni, N-codope d CoP/carbon fiber hybrids with improving reaction kinetics for superior sodium storage

Huijun Li et al.

Summary: The research presents a new synthesis strategy for a novel self-supporting anode material, demonstrating improved sodium storage performance by combining nickel, nitrogen co-doped graphitized carbon and cobalt phosphide embedded in carbon fiber, addressing issues such as volume expansion and poor electronic conductivity of transition-metal phosphides, achieving outstanding electrochemical performance.

JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY (2022)

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Article Materials Science, Multidisciplinary

3D printing interface-modified PDMS/MXene nanocomposites for stretchable conductors

Mathias Aakyiir et al.

Summary: This study developed and modified a Ti3C2 MXene ink with a siloxane surfactant, which showed strong interactions with a polydimethylsiloxane (PDMS) matrix. The resulting nanocomposite conductor exhibited high flexibility, conductivity, and mechanical resilience, providing a potential solution for applications in stretchable electronics and sensors.

JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY (2022)

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Article Chemistry, Physical

Highly reversible lithium metal-organic battery enabled by a freestanding MXene interlayer

Qikun Zhang et al.

Summary: Organic materials have attracted great interest as promising electrode materials for next generation batteries due to their abundant resources, environmental friendliness and rich functional groups. However, their development is impeded by the fast capacity decay caused by the high solubility of organic electrodes in liquid electrolyte. In this study, a free-standing MXene paper was introduced as an interlayer for the first time to overcome this issue. The MXene interlayer successfully blocked the dissolution of the cathode, leading to significantly enhanced capacity retention in the configured cells. The performance enhancing mechanism of the MXene interlayer was also investigated.

JOURNAL OF POWER SOURCES (2022)

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Article Chemistry, Physical

Hierarchical utilization of raw Ti3C2Tx MXene for fast preparation of various Ti3C2Tx MXene derivatives

Shunlong Zhang et al.

Summary: This study successfully achieved large-scale preparation of various derivatives of multilayered Ti3C2Tx MXene using a classified preparation strategy, including few-layered Ti3C2Tx powders, films, and nanowires. The utilization and processing efficiency of raw MXenes were improved through step-by-step delamination and solution-phase flocculation techniques.

NANO RESEARCH (2022)

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Super-Assembled Hierarchical and Stable N-Doped Carbon Nanotube Nanoarrays for Dendrite-Free Lithium Metal Batteries

Li Qiao et al.

Summary: In this study, stable 3D lithium metal anodes were prepared by growing N-doped carbon nanotubes on carbon cloth. The presence of carbon nanotubes effectively reduced the local current density and inhibited the formation of dendrites, leading to steady voltage curves and excellent cycle stability.

ACS APPLIED ENERGY MATERIALS (2022)

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Article Chemistry, Physical

Enhanced stability of Ti3C2Tx MXene enabled by continuous ZIF-8 coating

Eunji Choi et al.

Summary: MXenes have gained significant interest due to their outstanding properties and performance. However, their hydrophilic and metastable surfaces make most MXenes prone to oxidation, which can degrade their properties and hinder practical applications. In this study, the stability of Ti3C2Tx MXene films was enhanced by coating a continuous layer of zeolitic imidazolate framework-8 (ZIF-8). The enhanced stability can be attributed to the hydrophobic microporous structure of ZIF-8, which effectively hinders water permeation.

CARBON (2022)

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Review Polymer Science

A review of etching methods of MXene and applications of MXene conductive hydrogels

Can Zhou et al.

Summary: This paper reviews the etching methods, synthesis strategies and applications of MXene, and provides an outlook on its future development.

EUROPEAN POLYMER JOURNAL (2022)

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Article Chemistry, Physical

Fast-charging and dendrite-free lithium metal anode enabled by partial lithiation of graphene aerogel

Yong Ma et al.

Summary: This study presents a novel design of lithium metal anode, which effectively addresses the issue of dendrite growth in lithium metal batteries, leading to remarkable cycling performance and rate capability. It paves the way for the ultimate deployment of lithium metal batteries in real-world applications that require fast charging and deep cycling.

NANO RESEARCH (2022)

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Boron-doped three-dimensional MXene host for durable lithium-metal anode

Na Wu et al.

RARE METALS (2022)

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Vertically Aligned MXene Nanosheet Arrays for High-Rate Lithium Metal Anodes

Qian Chen et al.

Summary: In this study, vertically aligned Ti3C2Tx MXene nanosheet arrays were used to regulate Li metal nucleation and deposition, resulting in high Coulombic efficiencies and stability.

ADVANCED ENERGY MATERIALS (2022)

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Review Chemistry, Applied

The roles of MXenes in developing advanced lithium metal anodes

Nicolas Lucero et al.

Summary: This article provides an overview of the recent advances in the roles of MXenes for stabilizing lithium metal anodes. MXenes, with their excellent properties, have been used to address the issues in lithium metal anodes and offer new strategies for developing stable and dendrite-free lithium metal anodes.

JOURNAL OF ENERGY CHEMISTRY (2022)

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Article Chemistry, Physical

High utilization lithium metal anode constructed by allocatable MXene foam container

Mengli Tao et al.

Summary: This study proposes an allocatable container constructed with porous MXene and carbon nanofibers to restrain Li deposition behavior and improve the utilization of lithium metal anode. The experimental results demonstrate that this container provides fast mass transfer ability and good deposition behavior, effectively prolonging the battery's lifespan.

JOURNAL OF POWER SOURCES (2022)

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Article Engineering, Environmental

Nanoconfined SnS2 in robust SnO2 nanocrystals building heterostructures for stable sodium ion storage

Xiaoqin Cheng et al.

Summary: Transition-metal dichalcogenides are attractive host materials for Na+ insertion due to their high theoretical specific capacity, but their low conductivity and large volume fluctuations limit their practical applications. By introducing a more robust material and constructing a heterostructure, the internal stress and volume variations induced by Na+ insertion can be effectively cushioned, leading to improved structural stability and cycling performance.

CHEMICAL ENGINEERING JOURNAL (2022)

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Article Chemistry, Physical

MXene, silicene and germanene: preparation and energy storage applications

Adeel Zia et al.

Summary: Energy storage devices require low cost, easily prepared, high performing, light-weight and environment friendly materials. Two-dimensional nanomaterials like MXene, silicene and germanene have shown potential for energy storage applications due to their atomic thickness, large surface area and infinite planer distance.

MATERIALS TODAY ENERGY (2022)

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Synergistically engineered 2D MXenes for metal-ion/Li-S batteries: Progress and outlook

N. Iqbal et al.

Summary: MXenes, a class of two-dimensional materials, have exceptional properties that make them suitable for energy storage devices. MXene-based films exhibit outstanding ion storage and electron transport capabilities, making them ideal for metal-ion and Li-S batteries. These films outperform conventional electrode materials in terms of flexibility and functionality. This review provides an overview of recent advancements and methodologies in the design and manufacture of MXene films for metal-ion and Li-S batteries.

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Fast charging of energy-dense lithium-ion batteries

Chao-Yang Wang et al.

Summary: Researchers have achieved fast charging of high-energy density batteries using an asymmetric temperature modulation and a thermally stable dual-salt electrolyte method, allowing for a 75% state of charge in just 12 minutes. They have also developed a digital twin to assess cooling and safety, demonstrating the feasibility of thermally modulated 4C charging with air convection.

NATURE (2022)

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Conductive Iodine-Doped Red Phosphorus Enabled Dendrite-Free Lithium Deposition on MXene Matrix

Zhaolin Na et al.

Summary: Lithium metal has the potential to be used in next-generation batteries due to its high theoretical capacity and low redox potential. However, uncontrollable dendrite growth and volume change of lithium hinder its real-world application. In this study, a flexible MXene@iodine-doped red phosphorus paper is designed to enable dendrite-free lithium deposition. The iodine doping improves the conductivity of red phosphorus, promoting uniform lithium deposition and suppressing dendrite growth. The layered structure of conductive MXene paper provides ion transport channels and free spaces, alleviating the structural damage caused by volume change. The MXene@RP paper with preloaded lithium demonstrates long-term cycling stability.

SMALL (2022)

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Review Electrochemistry

Designing Lithium Argyrodite Solid-State Electrolytes for High-Performance All-Solid-State Lithium Batteries

Chongxing Li et al.

Summary: This review summarizes the basic physical and chemical properties, material synthesis strategies, chemical or electrochemical stabilities, and interface engineering of lithium argyrodite solid-state electrolytes in all-solid-state lithium batteries. It also provides an overview of recent achievements and critical challenges, as well as prospects for integrating lithium argyrodite SSEs into ASSLBs.

BATTERIES & SUPERCAPS (2022)

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Article Nanoscience & Nanotechnology

Three-Dimensional (3D) Nanostructured Skeleton Substrate Composed of Hollow Carbon Fiber/Carbon Nanosheet/ZnO for Stable Lithium Anode

Xue-Liang Zhang et al.

Summary: By investigating the mechanism of formation of a novel 3D nanostructured substrate, a stable environment for lithium metal deposition and stripping was proposed, preventing the generation of lithium dendrites effectively.

ACS APPLIED MATERIALS & INTERFACES (2021)

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Article Engineering, Environmental

Constructing ultrafine lithiophilic layer on MXene paper by sputtering for stable and flexible 3D lithium metal anode

Yi Qian et al.

Summary: A 3D flexible MXene@Au host has been designed to address the issue of lithium dendrite growth in lithium metal batteries, showing significantly improved performance with high capacity retention even after 200 cycles.

CHEMICAL ENGINEERING JOURNAL (2021)

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Article Chemistry, Multidisciplinary

Ultrafast, One-Step, Salt-Solution-Based Acoustic Synthesis of Ti3C2 MXene

Ahmed El Ghazaly et al.

Summary: This study presents a one-step synthesis method for the conversion from Ti3AlC2 MAX to Ti3C2Tz MXene on the order of milliseconds, facilitated by the combination of protons and fluorine ions to selectively etch the MAX phase. The results demonstrate that flexible electrodes fabricated using this method exhibit comparable electrochemical performance to previously reported ones.

ACS NANO (2021)

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Article Materials Science, Multidisciplinary

Two-dimensional transition metal carbides and/or nitrides (MXenes) and their applications in sensors

R. Qin et al.

Summary: MXenes have attracted great attention due to their excellent electrical conductivity, good hydrophilicity, excellent mechanical properties, large and adjustable interlayer spacing, rich surface functional groups, and large specific surface area. They are ideal materials for sensor applications and have been applied in various sensor fields.

MATERIALS TODAY PHYSICS (2021)

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Article Chemistry, Physical

Silicious nanowires enabled dendrites suppression and flame retardancy for advanced lithium metal anodes

Yujing Liu et al.

Summary: By designing a three-dimensional network structure with high specific surface area, strong electrolyte affinity, and flame-retardant properties, the safety hazards caused by dendritic Li plating in lithium metal batteries can be reduced, leading to dendrite-free Li deposition and improved cycle performance and safety.

NANO ENERGY (2021)

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Review Chemistry, Multidisciplinary

Advances in the Synthesis of 2D MXenes

Yi Wei et al.

Summary: MXenes, versatile materials with adjustable structures and rich surface chemistry, have been recognized as potential 2D materials for various applications. Recent research has focused on synthetic routes, etching methods, and delamination strategies for large-scale preparation and stable storage. Antioxidation strategies for MXenes have also been summarized for future developments and practical applications.

ADVANCED MATERIALS (2021)

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Review Chemistry, Applied

Lithium metal batteries for high energy density: Fundamental electrochemistry and challenges

Mingda Gao et al.

Summary: The dependence on portable devices and electric vehicles has led to a growing awareness of energy storage systems with high energy density, leading to a revival of interest in lithium metal batteries (LMBs). However, the growth of lithium dendrite during the electro-chemical process presents challenges for LMBs application, limiting Coulombic efficiency and causing safety issues. Understanding the mechanisms of lithium nucleation and dendrite growth is essential for addressing these challenges.

JOURNAL OF ENERGY CHEMISTRY (2021)

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Article Energy & Fuels

A high-energy-density and long-life initial-anode-free lithium battery enabled by a Li2O sacrificial agent

Yu Qiao et al.

Summary: Anode-free batteries are promising for high-energy applications, but face challenges with cycling stability due to limited lithium sources. In this study, researchers preloaded Li2O onto the cathode of an initial-anode-free cell to provide additional lithium for offsetting irreversible lithium loss during long-term cycling. By utilizing O-2(-) species released through Li2O oxidation and a fluorinated ether additive, a LiF-based layer was constructed at the cathode/electrolyte interface to passivate the cathode surface and inhibit the detrimental oxidative decomposition of ether solvents. As a result, a long-life 2.46 Ah initial-anode-free pouch cell with a gravimetric energy density of 320 Wh kg(-1) was achieved, maintaining 80% capacity after 300 cycles.

NATURE ENERGY (2021)

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Review Chemistry, Physical

Multifunctional roles of carbon-based hosts for Li-metal anodes: A review

Xiaolin Yan et al.

Summary: The paper discusses the critical role of carbon-based hosts in improving the performance of Li-metal anodes, analyzing the main failure mechanisms of Li-metal anodes and the advantages and strategies of carbon-based hosts in addressing challenges. It also reviews the functions, limitations, and recent research progress of key carbon-based host materials for Li-metal anodes, providing an outlook on the potential of carbon-based hosts in future research.

CARBON ENERGY (2021)

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Review Electrochemistry

High-Mass-Loading Electrodes for Advanced Secondary Batteries and Supercapacitors

Feng Wu et al.

Summary: The increasing demand for high energy density advanced electrochemical energy storage systems (EESSs) for electric vehicles and portable electronics is driving the electrode revolution, with the development of high-mass-loading electrodes (HMLEs) as a promising approach. However, HMLEs face challenges such as poor charge kinetics, electrode structural stability, and complex production processes. This review provides a comprehensive summary of HMLEs, discussing strategies to improve their electrochemical performance and their applications in various EESSs.

ELECTROCHEMICAL ENERGY REVIEWS (2021)

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The use of in-situ Raman spectroscopy in investigating carbon materials as anodes of alkali metal-ion batteries

Xiao-qin Cheng et al.

Summary: Raman spectroscopy is a powerful tool for studying phase transitions induced by temperature, pressure, or electrochemical reactions, and for tracking microstructural changes in electrode materials during charging and discharging. It is widely used to understand the energy storage mechanisms in lithium-ion batteries with carbon anode materials.

NEW CARBON MATERIALS (2021)

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Perpendicular MXene Arrays with Periodic Interspaces toward Dendrite-Free Lithium Metal Anodes with High-Rate Capabilities

Zhenjiang Cao et al.

ADVANCED FUNCTIONAL MATERIALS (2020)

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Single Zinc Atoms Immobilized on MXene (Ti3C2Clx) Layers toward Dendrite-Free Lithium Metal Anodes

Jianan Gu et al.

ACS NANO (2020)

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ELECTROCHIMICA ACTA (2020)

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Cheng-Lin Yan

RARE METALS (2020)

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A general Lewis acidic etching route for preparing MXenes with enhanced electrochemical performance in non-aqueous electrolyte

Youbing Li et al.

NATURE MATERIALS (2020)

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In situ surface protection of lithium metal anode in Lithium-Selenium disulfide batteries with ionic liquid-based electrolytes (vol 69, 104434, 2020)

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Recent Advances of Emerging 2D MXene for Stable and Dendrite-Free Metal Anodes

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Two-dimensional fluorine-free mesoporous Mo2C MXene via UV-induced selective etching of Mo2Ga2C for energy storage

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3D printing dendrite-free lithium anodes based on the nucleated MXene arrays

Kai Shen et al.

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Element Replacement Approach by Reaction with Lewis Acidic Molten Salts to Synthesize Nanolaminated MAX Phases and MXenes

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Two-Dimensional Ti3C2TX/CMK-5 nanocomposite as high performance anodes for lithium batteries

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In situ synthesis of CNTs@Ti3C2 hybrid structures by microwave irradiation for high-performance anodes in lithium ion batteries

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Fluoride-Free Synthesis of Two-Dimensional Titanium Carbide (MXene) Using A Binary Aqueous System

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Flexible Ti3C2 MXene-lithium film with lamellar structure for ultrastable metallic lithium anodes

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Guidelines for Synthesis and Processing of Two-Dimensional Titanium Carbide (Ti3C2TX MXene)

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Preparation of Ti3C2 and Ti2C MXenes by fluoride salts etching and methane adsorptive properties

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Toward Safe Lithium Metal Anode in Rechargeable Batteries: A Review

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