☆ 4.7 Review

Radical and (photo)electron transfer induced mechanisms for lignin photo- and electro-catalytic depolymerization

GREEN ENERGY & ENVIRONMENT (2023)

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Summary: This study provides a new perspective on the pyrolysis of lignin and polyethylene, revealing the role of polyethylene in promoting the formation of phenolic monomers. The findings show that the interaction between lignin and polyethylene is crucial for improving the yields of lignin-derived products. Mass transfer plays a significant role in controlling the interactions, as confirmed by experimental analysis.

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Summary: This review evaluates the technical readiness level of photoelectrocatalysis (PEC) techniques for wastewater treatment and energy recovery, with a focus on the pulp and paper (P&P) industry. Experimental parameters play a crucial role in the removal of organic pollutants and energy recovery through PEC performance metrics. Additionally, cost analysis, energy consumption, and durability present critical challenges in enhancing PEC technologies.

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Summary: The study presents an efficient electrocatalytic strategy for cleaving C-alpha-C-beta bonds in lignin model compounds at room temperature using platinum as the anode and tert-butyl hydroperoxides as the oxidants, resulting in high yields of aromatic aldehydes and phenols. This electrocatalytic strategy is highly selective and can transform a wide range of lignin models and polymers into desired aromatic aldehydes. Mechanistic studies suggest that the reaction proceeds via a C-beta radical process involving a peroxide intermediate, showing potential for using renewable electricity to selectively break C-alpha-C-beta bonds and transform lignin into valuable chemicals under ambient conditions.

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Oxidation of organosolv lignin in a novel surfactant-free microemulsion reactor

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Summary: A surfactant-free microemulsion reactor was designed to enhance the oxidative depolymerization of lignin, resulting in a substantial improvement in phenolic monomer yield. This intensification was rationalized by the solubilization effect of the microemulsion system and directional aggregation of lignin at the microemulsion interface.

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Summary: The rapid development of radical chemistry has led to the emergence of innovative strategies for organic synthesis, among which photoelectrocatalysis (PEC) has received considerable attention as a promising approach. Although many catalytic reactions face challenges such as high overpotential and poor conversion efficiency, scientists are actively seeking solutions to enhance the accessibility and further development of photoelectrocatalytic technology for specific chemical bond formation and catalytic system fabrication.

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Summary: Electrocatalytic processes in organic chemistry have garnered renewed interest, particularly as an alternative to conventional synthetic methods when coupled with renewable feedstocks. The development of selective degradation methods for lignin is crucial for synthesizing simpler aromatic hydrocarbons from the largest natural source of aromatic rings.

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Summary: Electrocatalytic lignin upgrading powered by renewable electricity enables decentralized production of chemicals and fuels under gentle conditions. This field faces challenges but has promising future prospects.

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Summary: In this study, cleavage of aryl ether (C-aryl-O) bonds in lignin model compounds was achieved through electrocatalytic oxidation under mild conditions, and the oxidation mechanism was fully explored. By optimizing the ionic liquid system and studying the effects of N-2/O-2 atmospheres, some insights were provided for efficient utilization of lignin under mild conditions.

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Summary: The cleavage of linkage bonds among the C9 units in lignin molecules via selective oxidation method is an important process for lignin valorization. This study investigated the cleavage pathways of bonds in a lignin model compound by reactive oxygen species (ROS) generated through electrochemical oxygen reduction reaction in an aprotic ionic liquid, showing that different ROS led to different cleavage pathways.

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