☆ 3.8 Review

Pore network characterization of shale reservoirs through state-of-the-art X-ray computed tomography: A review

GAS SCIENCE AND ENGINEERING (2023)

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3D visualization of tectonic coal microstructure and quantitative characterization on topological connectivity of pore-fracture networks by Micro-CT

Kaizhong Zhang et al.

Summary: Research on the connectivity characteristics and topological relationships of pore-fracture networks in coal is crucial for understanding the microstructure evolution. Micro-CT technology was used to characterize the microstructure of original, tectonic, and reconstructed coals, revealing the impact of tectonism and external stress loading on coal microstructure evolution. Tectonic coal exhibited significantly increased pore space connectivity compared to original coal, while reconstructed coal showed a decrease in connectivity after stress loading.

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Article Energy & Fuels

Effects of pore connectivity and water saturation on matrix permeability of deep gas shale

Jiale Zhao et al.

Summary: This study evaluated the permeability of deep shales in the Yichang area, Middle Yangtze using three methods and found significant differences in horizontal and vertical permeability. Microfractures and laminae were identified as the dominant gas transport channels, and increasing water saturation led to a decrease in matrix permeability.

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Article Thermodynamics

Changes of pore structures and permeability of the Chang 73 medium-to-low maturity shale during in-situ heating treatment

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Summary: The study investigates the permeability changes and their relationship with the microstructure in shale cores from the Chang 73 sub-member shale oil reservoir under different temperatures and stresses. The experimental results demonstrate that the porosity and permeability can be significantly increased when the temperature exceeds 400 degrees C. Furthermore, the coverage and connectivity of the fracture network are greatly improved. Kerogen pyrolysis is identified as the primary mechanism leading to remarkable improvements in microstructure and physical properties.

ENERGY (2022)

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Article Energy & Fuels

Pore accessibility by wettable fluids in overmature marine shales of China: Investigations from contrast-matching small-angle neutron scattering (CM-SANS)

Mengdi Sun et al.

Summary: The characterization of pore accessibility in shale oil and gas reservoirs is essential but challenging. This study used contrast-matching small-angle neutron scattering (CM-SANS) and other experiments to investigate nanoscale pore accessibility characteristics and their controlling factors in overmature marine shale samples. A novel accessibility index was developed and used to analyze the accessibility of different wetting phases in nanoscale pore networks. The results showed that toluene filled higher pore volumes (>7 nm) due to the development of organic pores and their connection with inorganic pore systems, while water-accessible pores were observed within a pore size of less than 7 nm. The accessibility to water and toluene was controlled by pore surface wettability and pore connectivity. CM-SANS is an effective means of evaluating nanoscale pore accessibility in shale.

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Article Energy & Fuels

U-Net model for multi-component digital rock modeling of shales based on CT and QEMSCAN images

Bingke Li et al.

Summary: This paper presents a method to accurately and quickly establish digital core images with multi-mineral components. By training a U-Net model, the CT images are automatically segmented and converted into multi-mineral component images, and manually segmented micropores and fractures are added. The results are satisfactory.

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Reconstruction of the microstructure based on hierarchical simulated annealing with erosion method

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Summary: The microstructure of porous media has a direct impact on its macroscopic properties, such as conductivity and transport properties. This paper proposes a novel modeling scheme that can reconstruct more accurate microstructures. The effectiveness of the proposed method is demonstrated through comparisons with original images.

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Flow simulation considering adsorption boundary layer based on digital rock and finite element method

Yong-Fei Yang et al.

Summary: Due to the low permeability of tight reservoirs, throats are crucial in controlling fluid flow. This study investigates the effects of adsorption boundary layer (ABL) on fluid flow in throats using digital rock method, showing that the viscosity and thickness of ABL significantly hinder fluid flow.

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Time-resolved grain-scale 3D imaging of hydrofracturing in halite layers induced by gypsum dehydration and pore fluid pressure buildup

S. Marti et al.

Summary: This study investigated the role of gypsum dehydration in the deformation of evaporitic rocks and found that the fluid released by dehydrating gypsum accumulates at the gypsum-halite interface. The experiment results indicate that impermeable halite layers in evaporites are unlikely to trap overpressured fluid and dehydration reactions alone may not explain intermediate depth seismicity in subduction zones. The data demonstrate the significant potential of in-situ 4D imaging for investigating fundamental tectonic processes at the grain scale.

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In-situ synchrotron characterisation of fracture initiation and propagation in shales during indentation

Lin Ma et al.

Summary: The feasibility and advantages of synchrotron imaging in characterizing fracture initiation and propagation in shales during indentation tests have been demonstrated. Experimental studies on different variables of shale microstructure were conducted, successfully capturing the evolution of fractures through imaging experiments.

ENERGY (2021)

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Article Geosciences, Multidisciplinary

Striving to translate shale physics across ten orders of magnitude: What have we learned?

Yashar Mehmani et al.

Summary: Shales will play a key role in the transition to renewable energy but face challenges due to their nanoporous structure and extreme heterogeneity. Challenges include understanding fluid flow and phase behavior in shales, and the lack of scale separation for reliable physics descriptions. Advances in computational power, imaging technology, and machine learning are helping to address these challenges through scale translation methods.

EARTH-SCIENCE REVIEWS (2021)

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Article Energy & Fuels

Experimental investigation on hydration mechanism of Sichuan shale (China)

Jingping Liu et al.

Summary: This study investigated the mechanisms of shale hydration and found that the high content of illite and absence of smectite in shale formations led to a rapid hydration process due to hydrogen bonding forces. In contrast to mudstone, shale showed a faster hydration rate, making conventional inhibitors ineffective in preventing shale rock hydration.

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Article Energy & Fuels

Controls on reservoir properties in organic-matter-rich shales: Insights from MICP analysis

Maria Mastalerz et al.

Summary: Mercury injection capillary pressure (MICP) analysis was used to study organic-matter-rich Devonian shales with varying maturity levels to discuss controls on drainage and imbibition in shale reservoirs. Results showed that maturity influences the pore size distribution, with higher-maturity samples having lower volumes of smaller pores.

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Article Energy & Fuels

A method for automatic shale porosity quantification using an Edge-Threshold Automatic Processing (ETAP) technique

Shansi Tian et al.

Summary: SEM is a prevalent method used for imaging and quantifying the pore size distribution of shale rock. A new ETAP method is introduced in this study for robust extraction and quantification of pore data, showing reliable results compared to traditional methods.

FUEL (2021)

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Article Thermodynamics

The effect of tectonic deformation and preservation condition on the shale pore structure using adsorption-based textural quantification and 3D image observation

Qiyang Gou et al.

Summary: The study shows that tectonism significantly impacts the pore characteristics of organic-rich shales. Shales from stable regions have better pore structure parameters compared to deformed region shales, resulting in higher shale gas yield. The research also provides 3D pore deformation information of shale reservoirs under complex tectonic episodes.

ENERGY (2021)

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Gas Flow Models of Shale: A Review

Farzam Javadpour et al.

Summary: Conventional flow models based on Darcy's flow physics are inadequate in accurately modeling shale gas production data, leading to the proposal of various gas-flow models specifically for shale reservoirs. The microscopic pores in shale, known as nanopores, primarily associated with organic matter, contribute to a dual pore system that increases the complexity of gas flow. In addition to viscous flow, shale's permeability results in gas slippage and Knudsen diffusion, adding more flow processes beyond Darcy's law.

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Experimental and numerical study of gas diffusion and sorption kinetics in ultratight rocks

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Summary: This study provides a quantitative analysis of gas transport behavior in ultratight rocks using X-ray computed micro-computed tomography imaging and numerical modeling. The results show that sorption is a non-equilibrium process in ultratight rocks and surface diffusion significantly contributes to total mass transport through nanopores.

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Characterization of Closed Pores in Longmaxi Shale by Synchrotron Small-Angle X-ray Scattering

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Summary: The study systematically characterized the closed pores of Longmaxi Formation shale in Sichuan Basin by combining small-angle X-ray scattering with two fluid intrusion methods. Factors such as TOC content and mineral composition were found to affect the development of closed pores in the shale, while a relationship between shale matrix permeability and the fraction of closed pores was indirectly observed. Additionally, the fractal dimension of the system was deduced to be influenced by the closed pores, indicating potential for increased oil and gas production and recovery rates through further opening of the closed system during shale gas development.

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Summary: Quantitative characterization of shale gas flow in fractured shale is essential in shale gas extraction. This study reconstructed 3D multi-scale structures in fractured shale using various techniques and analyzed the effects of fracture complexity and gas pressure on shale gas flow quantitatively. The results showed that fracture morphology and gas pressure greatly influenced gas flow behavior in fractured shale.

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A comprehensive analysis of the pyrolysis effects on oil shale pore structures at multiscale using different measurement methods

Jian Lei et al.

Summary: The study evaluated the effects of pyrolysis on the pore structure of oil shale through experiments and analysis, showing that pyrolysis significantly increases porosity and changes pore sizes. The results suggest that a single pore detection method has limitations and multiple methods need to be integrated to understand the pore structures of oil shale.

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Article Energy & Fuels

Integration of Multiscale Imaging of Nanoscale Pore Microstructures in Gas Shales

Mohamed Garum et al.

Summary: Quantification of shale microstructures across a wide range of scales is challenging due to the complexity of the material. This study employed various techniques such as nano-CT, MIP, and nitrogen adsorption to analyze the microstructure of a gas shale sample, revealing differences in porosity and kerogen fraction measurements. The results suggest high shale gas potential based on pore size distribution, aspect ratio, and permeability assessments.

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Review Energy & Fuels

Application of nuclear magnetic resonance (NMR) in coalbed methane and shale reservoirs: A review

Zhengshuai Liu et al.

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Multiscale characterization of pore structure and connectivity of Wufeng-Longmaxi shale in Sichuan Basin, China

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Organic matter pores structure and evolution in shales based on the he ion microscopy (HIM): A case study from the Triassic Yanchang, Lower Silurian Longmaxi and Lower Cambrian Niutitang shales in China

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Formation and evolution of nanopores in shales and its impact on retained oil during oil generation and expulsion based on pyrolysis experiments

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Full-scale pores and micro-fractures characterization using FE-SEM, gas adsorption, nano-CT and micro-CT: A case study of the Silurian Longmaxi Formation shale in the Fuling area, Sichuan Basin, China

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Multifractal characteristics of Longmaxi Shale pore structures by N-2 adsorption: A model comparison

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Multiscale Description of Shale Pore Systems by Scanning SAXS and WAXS Microscopy

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Experimental study of anisotropic gas permeability and its relationship with fracture structure of Longmaxi Shales, Sichuan Basin, China

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Heterogeneous nanoporosity of the Silurian Longmaxi Formation shale gas reservoir in the Sichuan Basin using the QEMSCAN, FIB-SEM, and nano-CT methods

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