期刊
RSC ADVANCES
卷 6, 期 32, 页码 27004-27007出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ra00267f
关键词
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资金
- Natural Science Foundation of China [21506177]
- Natural Science Foundation of Fujian Province of China [2015J05034]
- Fujian province development and reform commission
- Key Program for Cooperation between Universities and Enterprises in Fujian Province [2013N5011]
- Fundamental Research Funds for the Xiamen University [20720160077]
5-Chloromethylfurfural (5-CMF), a biomass-derived platform chemical with great potential applications, was synthesized by a novel method from sugars, using metal chlorides as catalysts in a deep eutectic solvent (DES). AlCl3 center dot 6H(2)O was verified as the most effective catalyst among various metal chlorides, and provided a 5-CMF yield of 50.3% along with 8.1% 5-HMF yield at 120 degrees C in 5 h. By this green, mild and cost-effective approach, the dependence of 5-CMF production on the large amount and high concentration of hydrochloric acid in previous studies was eliminated.
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