期刊
RSC ADVANCES
卷 6, 期 25, 页码 20588-20597出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ra03447k
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资金
- Department of Science and Technology-Science and Engineering Research Board (DST-SERB), New Delhi [SB/S1/OC-39/2014]
- CSIR, New Delhi
A simple and efficient method for the synthesis of xanthenes and dihydroacridines containing a quaternary carbon atom at the 9th-position, is presented. Significantly, the protocol facilitated the smooth participation of sterically hindered and protecting group free 2-bromobenzyl tertiary alcohols in cross coupling reactions with phenols and anilines, under copper-catalysis. The Lewis acid mediated intramolecular C-C bond formation enabled the formation of a quaternary carbon atom at the 9th-position. Remarkably, this two-step protocol required a single column purification technique.
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