期刊
ARABIAN JOURNAL OF CHEMISTRY
卷 9, 期 -, 页码 S1740-S1746出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.arabjc.2012.04.046
关键词
N,O-Bis(trimethylsilyl)acetamide; Dicyclohexyl carbodimide; Solvent free; 3,4-Dihydropyrimidinones; 3,4-Dihydropyrimidithiones
We report herein, the usage of N,O-bis(trimethylsilyl) acetamide (BSA) and dicyclohexyl carbodimide (DCC) as two new catalysts for three component condensation of an aldehyde, ethyl acetoacetate and urea/thiourea under solvent free conditions at 100 degrees C to afford the corresponding 3,4-dihydropyrimidine-2-(1H)-ones/thiones (DHPMs) in good to excellent yields. A comparative study of these two catalysts was made and presented. (C) 2012 Production and hosting by Elsevier B.V. on behalf of King Saud University.
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