期刊
SYNTHESIS-STUTTGART
卷 49, 期 5, 页码 1103-1108出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0036-1588616
关键词
nitration; dinitrogen pentoxide; nitramides; nitramines; 1,1,1,2-tetrafluoroethane
资金
- Russian Foundation of Basic Research [13-03-12223, 16-29-01042]
A convenient one-pot synthesis of primary aliphatic N-nitramines, which includes the nitration of available N,N'-dialkyloxalamides or N-alkylcarbamates with dinitrogen pentoxide in the 1,1,1,2-tetrafluoroethane media followed by ammonolysis of intermediate N-nitroamides in the same solvent has been developed. The method is environmentally safe, and affords target N-nitramines in up to 94% overall yield.
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