期刊
ORGANIC LETTERS
卷 18, 期 19, 页码 5030-5033出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b02488
关键词
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资金
- MEXT
- JSPS KAKENHI [JP16H01161, JP16K05781]
- Grants-in-Aid for Scientific Research [16K05781, 16H01161] Funding Source: KAKEN
1,2-cis-alpha-Stereoselective glycosylations were conducted using a 1,2-anhydroglucose donor and mono-ol acceptors in the presence of a glycosyl-acceptor-derived borinic ester. Reactions proceeded smoothly under mild conditions to provide the corresponding alpha-glycosides with high stereoselectivity in moderate to high yields. In addition, the present method was applied successfully to the direct glycosylation of a protected ceramide acceptor and the total synthesis of natural glycosphingolipids (GSLs).
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