期刊
ORGANIC LETTERS
卷 18, 期 4, 页码 704-707出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.5b03672
关键词
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资金
- Australian Research Council
- Institute of Advanced Studies
- China Scholarship Council
The title natural product 1 has been synthesized by treating the 1,2,3,5-tetrasubstituted pyrrole 23 with oxoperoxymolybdenum(pyridine) (hexamethylphosphoric triamide) (MoOPH). Compound 23 was itself prepared in seven steps from parent pyrrole using Ullmann-Goldberg and Suzuki-Miyaura cross-coupling, Vilsmeier-Haack formylation, electrophilic bromination, and Wittig olefination reactions as key steps. Related chemistry has been used to prepare discoipyrrole B (2).
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