期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 14, 期 28, 页码 6679-6682出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ob01069e
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资金
- Biomolecular Interaction Centre
- University of Canterbury
Unprotected carbohydrates can be directly converted into cyanomethyl thioglycosides in a completely stereoselective manner by reaction with 2-chloro-1,3-dimethylimidazolinium chloride (DMC) and mercaptoacetonitrile in aqueous solution in the presence of triethylamine. Reaction with methoxide provides 2-imino-2-methoxyethyl (IME) thioglycosides, which may be used directly for the glycosylation of surface protein lysine residues.
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