期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 357, 期 14-15, 页码 3141-3147出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201500628
关键词
cycloisomerization; flow chemistry; gold nanoparticles; green chemistry; heterogeneous catalysis
资金
- Agency for Innovation by Science and Technology (IWT)
- CatchBio
A continuous-flow protocol for the gold-catalyzed cycloisomerization of sterically hindered Ugi-adducts to spiroindolines in a packed-bed reactor is presented. Spiroindolines with various substitution patterns are formed in good yields and with good selectivity. A detailed characterization of the catalyst deactivation process was conducted, whereas no metal leaching from the catalyst was detected.
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