期刊
ADVANCED SYNTHESIS & CATALYSIS
卷 357, 期 4, 页码 714-718出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201400785
关键词
copper; N,N-dimethylanilines; N-methylanilines; room-temperature arylation; water
资金
- National Natural Science Foundation of China [21202041]
- Key Discipline Project of Hunan Province
The first room-temperature copper-catalyzed arylations of dimethylamine and methylamine in neat water have been developed. Using a combination of CuI and 6,7-dihydroquinolin-8(5H)-one oxime as catalyst, dimethylamine is arylated with various aryl halides to give the corresponding products in good to excellent yields. Further, this catalysis enables the selective arylation of methylamine to afford the high yields of monoarylated methylamines as the sole products.
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