Influence of SiC nanoparticle contents on microstructural evolution and mechanical behavior of AZ91D magnesium matrix composites synthesised through a combination of a master pellet feeding technique and stir casting assisted by ultrasonic vibration

In this current study, an integrated approach involving a master pellet feeding technique and stir casting assisted by ultrasonic treatment processing was employed to fabricate AZ91D magnesium matrix nanocomposites reinforced with various concentrations of SiC nanoparticles (1.0, 1.5, and 2.0 wt%). The influence of the nanoparticle feeding method and the weight fraction of reinforcement on the microstructure and mechanical properties of AZ91D/SiC composites was thoroughly examined. The microstructural analysis revealed that the implementation of a master pellet feeding approach resulted in a relatively uniform dispersion of SiC nanoparticles within the primary & alpha;-Mg phase, whereas the original nanoparticle feeding method led to noticeable particle agglomeration in the microstructure. Additionally, with an increasing weight fraction of SiC nanoparticles, the primary & alpha;-Mg grain became finer and the & beta;-Mg17Al12 intermetallic phase turned smaller. The hardness and tensile properties of AZ91D/SiC composites were significantly enhanced with increasing SiC contents. The addition of 2.0 wt% SiC reinforcements to the AZ91D magnesium alloy resulted in a maximal hardness increase of 41 %. Nevertheless, the ultimate tensile strength (UTS) and elongation (%EL) decreased when the SiC content exceeded 2.0 wt% due to the presence of increased porosity content and particle clusters in the microstructure. Notably, the AZ91D/ 1.5 wt% SiC composite exhibited promising tensile properties, with yield strength (YS), ultimate tensile strength (UTS), and elongation (%EL) values of 151 MPa, 192 MPa, and 4.54 %, respectively.

Automated summary

In this study, AZ91D magnesium matrix nanocomposites reinforced with SiC nanoparticles were fabricated using a master pellet feeding technique and stir casting with ultrasonic treatment. The microstructure and mechanical properties of the composites were investigated. The use of a master pellet feeding approach resulted in a more uniform dispersion of SiC nanoparticles, while the original nanoparticle feeding method led to particle agglomeration. Increasing the SiC content improved the hardness and tensile properties of the composites, but excessive SiC content caused a decrease in ultimate tensile strength and elongation due to increased porosity and particle clusters.