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Article
Chemistry, Physical
Milad Rasouli et al.
Summary: The incorporation of ZnO in HZSM-5 zeolites was achieved through five different methods, and the influence of these methods on the performance of ZnO/HZSM-5 catalysts in the direct hydrogenation of CO2 to aromatics was evaluated. The introduction of ZnO led to a decrease in surface area and micropore volume, except when ZnO was added to the synthesis gel. The high amount of Bronsted acidity was found to enhance CO2 conversion and aromatics synthesis, and the addition of ZnO decreased weak acid sites while increasing strong acid sites. The CO2 conversion followed a specific sequence, with the ZnO/ZSM-5-HS catalyst showing outstanding aromatics selectivity and CO2 conversion.
Article
Chemistry, Physical
Manikandan Krishnamurthy et al.
Summary: Hierarchical micro-mesoporous ZSM-5 zeolite was synthesized by using corn plant stem pith powder as a hard template. The addition of pith powder increased the porosity of the zeolites, resulting in better catalytic performance with higher conversion rate and selectivity in the formation of 2-Benzyl-1, 3, 5-trimethylbenzene. The presence of hierarchical pores and strong acidity in C-ZSM-5 contributed to its improved selectivity and stability.
Article
Energy & Fuels
Dan Yu et al.
Summary: Fe-doped ZSM-5 zeolite catalysts were studied for their activity and characteristics changes in the NH3 selective catalytic reduction of NOx. The results showed that the SCR activity was mainly dependent on active Fe species rather than acidity. Fe-oxo related Lewis sites played an important role in the low-temperature SCR reaction, while high Bronsted acidity was not necessary for high SCR activity. The study also revealed the conversion of inactive free Fe2+ ions to isolated Fe3+ species during high-temperature calcination and thermal aging, which was inhibited by water.
Article
Chemistry, Physical
Yuqian Liang et al.
Summary: Cu-exchanged SSZ-16 zeolite catalysts were modified with Ce to improve their hydrothermal stability. Increasing Ce contents significantly enhanced the stability, with CuCe0.87-SSZ-16 showing the best performance. Characterization measurements revealed that Ce modification strengthened the structural stability and increased the active Cu2+-2Z species, contributing to the improved hydrothermal stability.
Article
Engineering, Chemical
Junlin Xie et al.
Summary: MnOx and Sm-Mn catalysts prepared by coprecipitation method demonstrated excellent activities and sulfur resistances in the selective catalytic reduction of NOx by NH3 at temperatures between 50 and 300 degrees C with excess oxygen. 0.10Sm-Mn catalyst showed superior catalytic activity and sulfur resistance. The addition of Sm affected the phases, morphology structures, gas adsorption, reaction process, and specific surface areas, resulting in enhanced NO conversion, N-2 selectivity, and sulfur resistance. Extensive investigations were conducted on the reaction mechanism and the impact of SO2 on the catalysts.
FRONTIERS OF CHEMICAL SCIENCE AND ENGINEERING
(2023)
Article
Chemistry, Physical
Shiyu Xu et al.
Summary: MnOx catalysts with 3D structure (Mn-HT) were prepared using KIT-6 as a template by the hard-template method, and their catalytic performance for the selective catalytic reduction of NOx by NH3 was investigated at low temperatures. It was found that the template KIT-6 prepared at different hydrothermal temperatures significantly affected the catalytic performance of Mn-HT catalysts. Among them, Mn-140 catalyst prepared using the template obtained at a hydrothermal temperature of 140 degrees C exhibited the highest catalytic performance. Characterizations showed that Mn-140 catalyst possessed high reducibility with abundant surface oxygen species and Mn4+ species. NH3-TPD and in situ DRIFTS demonstrated that there were more Lewis acid sites and Bronsted acid sites on the surface of Mn-140 catalyst, promoting the adsorption and activation of NH3 and efficiently reducing NOx mainly by the Eley-Rideal (E-R) mechanism, accompanied by the Langmuir-Hinshelwood (L-H) mechanism.
APPLIED CATALYSIS A-GENERAL
(2023)
Review
Energy & Fuels
M. Sunil Kumar et al.
Summary: Emission plays a crucial role in air pollution and its impact on living organisms. Selective Catalytic Reduction (SCR) is a commonly used technology to reduce Nitrogen Oxides (NOx) emissions in internal combustion engines. This review examines various catalysts used in SCR, including metal-based catalysts and zeolite-based catalysts, and explores their performance and characteristics in terms of GHSV, efficiency at different temperature ranges, percentage doping, and NOx conversion efficiency. The review concludes that zeolite catalysts show excellent deNOx efficiency, with 2 to 4 wt% doping of Cu achieving around 95% deNOx and doping of Fe widening the operating temperature range.
Review
Chemistry, Physical
Boji Wang et al.
Summary: Increasingly stringent regulation towards nitrogen oxides (NOx) emission worldwide calls for efficient technologies such as selective catalytic reduction (SCR) with NH3. Transition metals supported on small-pore zeolites, especially Cu-SSZ-13, have been successfully applied to NOx abatement in road transport and can be extended to stationary sources. However, the stability and activity of such catalysts need to be revisited and tuned to accommodate the complex operating conditions in various industries. This review critically discusses the poisoning and deactivation mechanisms of zeolite-based SCR catalysts, aiming to establish the link between current catalysts and the demands in industries.
CHEMICAL PHYSICS IMPACT
(2023)
Article
Chemistry, Physical
Chenxin Su et al.
APPLIED SURFACE SCIENCE
(2023)
Article
Chemistry, Applied
Anqi Guo et al.
Summary: This paper summarizes recent advancements in the development and application of novel zeolites as selective catalytic reduction (SCR) catalysts for nitrogen oxides (NOx) abatement from lean-burn heavy-duty vehicles. It focuses on the synthesis, structure-performance relationship, and potential application of small-pore zeolites as catalysts in SCR with NH3 as the reductant. The post-synthetic modifications of small-pore zeolites, Cu-free small-pore zeolites, and mechanistic understandings of NH3-SCR chemistry over small-pore zeolite catalysts are also discussed, along with the potential of several novel small-pore zeolites for real application in NH3-SCR and the development of new SCR systems.
Article
Energy & Fuels
Shuo Feng et al.
Summary: A series of xSm-WZZ catalysts were prepared to improve the SO2 resistance and regeneration performance of diesel engine NH3-SCR catalysts. The 1Sm-WZZ catalyst exhibited the best SO2 and H2O resistance and slightly improved the NH3-SCR activity.
Article
Engineering, Environmental
Guanlin Huang et al.
Summary: NOx emission is a major cause of acid rain and photochemical smog, which have had a serious impact on the ecological environment, production, and daily life. Effective reduction of NOx emissions has become an important topic, with selective catalytic reduction (SCR) being the main research direction due to its high efficiency. Carbon-based materials, known for their large surface area, well-developed pore structure, and strong adsorption capacity, are widely used as catalyst carriers in SCR. This paper reviews recent research achievements in using activated carbon, carbon nanotube, graphene, and other carbon materials as SCR catalyst carriers, and summarizes the catalytic efficiency of these catalysts. The differences in properties due to different modification and preparation methods, as well as the effects of H2O and SO2 on the catalysts, are discussed. Challenges in the industrial application of carbon-based catalysts and future research directions are also highlighted.
JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING
(2023)
Article
Chemistry, Physical
Zhaoying Di et al.
Summary: By constructing a core-shell ZSM-5@CeO2 support and loading copper, the NH3-SCR performance, as well as the tolerance to H2O and SO2, was improved. The Cu/(ZSM-5@CeO2) catalyst showed superior activity with the lowest T-90 at 215°C, attributed to the interaction between CeO2 shell and copper ions, which enhanced the redox properties. The ZSM-5 core provided more acid sites for improved ammonia adsorption. The CeO2 shell preferentially reacted with SO2, leading to high sulfur tolerance. This study provides a strategy for designing and applying NH3-SCR zeolite catalysts.
APPLIED CATALYSIS A-GENERAL
(2022)
Article
Energy & Fuels
Heng Xie et al.
Summary: Manganese-doped FeVO4 catalysts were synthesized using a novel one-pot method, and the effect of Mn doping on FeVO4 in the selective catalytic reduction of NOx with NH3 was studied extensively. The 0.3Mn-FeV catalyst demonstrated superior deNOx performance, reaching 100% NOx conversion rate at 250 degrees C. Various characterization techniques revealed that Mn doping improved the crystal size, acidity, and redox properties of the catalyst, facilitating NH3 activation and maintaining V species in a higher oxidation state for enhanced performance in the SCR reaction.
Article
Chemistry, Inorganic & Nuclear
Jian Yang et al.
Summary: The La-doped Ce-Cu/Z5 catalyst demonstrated excellent SCR activity and stability in the selective catalytic reduction of NOx via ammonia. Its performance is attributed to the promotion of oxygen vacancy formation and optimization of the surface redox cycle, facilitating the efficient SCR reaction.
JOURNAL OF SOLID STATE CHEMISTRY
(2022)
Article
Chemistry, Applied
En-Hui Yuan et al.
Summary: Cu-Fe-ZSM-5 zeolites were prepared by hydrothermal synthesis using metal chelates embedded into the ZSM-5 crystals. The resulting materials exhibited ultra-small size and high dispersion, and showed excellent catalytic performance, stability, and tolerance.
MICROPOROUS AND MESOPOROUS MATERIALS
(2022)
Article
Chemistry, Physical
Pengfei Li et al.
Summary: This study reports the fabrication of a cobalt-doped trimetallic catalyst through pyrolysis of a metal-organic framework, which shows excellent performance in NH3 selective catalytic reduction, high water and sulfur resistance, and good stability. The results suggest the potential for developing a high stability catalyst for low-temperature selective catalytic reduction of NOx with NH3.
Article
Chemistry, Physical
Jie Yang et al.
Summary: Research shows that sulfur dioxide can have a dual effect on catalysts in the process of NH3-SCR of NO, both inhibiting the catalyst's low-temperature activity and enhancing N-2 selectivity. The presence of Fe species in the Mn-Fe/AC catalyst can improve selectivity and exhibit better sulfur resistance when exposed to SO2.
MOLECULAR CATALYSIS
(2022)
Article
Chemistry, Physical
Shufeng Shan et al.
Summary: The study demonstrates that the acid amount and crystallite size of microporous ZSM-5 are key factors affecting the hydrodealkylation (HDAK) performance of 1,3,5-trimethylbenzene (1,3,5-TMB). The presence of mesopores inside ZSM-5 facilitates the accessibility of 1,3,5-TMB to NiMoS and acid sites, improving the HDAK performance.
CATALYSIS SURVEYS FROM ASIA
(2022)
Review
Energy & Fuels
Pengju Wu et al.
Summary: Studying the alkali metal poisoning mechanism and antipoisoning measures of the SCR catalyst is crucial for increasing the service life of a catalyst and reducing the operation cost of a SCR denitration system.
Article
Chemistry, Physical
Hongyan Xue et al.
Summary: M/ZSM-5 (M = Mn, Co, Cu) samples were prepared by impregnation and their catalytic performance in NH3-SCR of NO was tested. Cu/ZSM-5 exhibited the highest activity, followed by Mn/ZSM-5, and Co/ZSM-5 was the least active. In-situ DRIFTS analysis revealed the nature and evolution of surface species. Coordinated NH3, NH4+, and amide (-NH2) species derived from NH3 adsorption were found to be relevant for NH3-SCR, while bridged nitrate species derived from NOx adsorption were identified as the main active species. Bridged nitrate was more abundant and thermally more stable on Cu/ZSM-5, consistent with its higher activity compared to Mn/ZSM-5 and Co/ZSM-5. Different mechanisms, including Eley-Rideal and Langmuir-Hinshelwood, were observed for Mn/ZSM-5 at different temperatures, while both pathways coexisted for Co/ZSM-5 and Cu/ZSM-5.
SURFACES AND INTERFACES
(2022)
Article
Engineering, Environmental
Shilin Zhao et al.
Summary: This paper comprehensively and systematically reviews the composition, deNOx characteristics, poisoning, and regeneration of commercial V2O5-WO3/TiO2 SCR catalyst, based on recent studies. It has important guiding significance for poisoning study and regeneration technology development of commercial SCR catalysts.
PROCESS SAFETY AND ENVIRONMENTAL PROTECTION
(2022)
Article
Chemistry, Multidisciplinary
Houda Jouini et al.
Summary: This study investigates the performance change of Fe-Cu-ZSM-5 SCR catalyst after contacting with poisoning species such as sodium and potassium. It is found that the introduction of alkali metals does not deteriorate the crystallinity and morphology of zeolite crystals, but leads to a significant loss of surface acidity, resulting in a dramatic deactivation of the SCR reaction.
RESEARCH ON CHEMICAL INTERMEDIATES
(2022)
Article
Energy & Fuels
Somayeh Taghavi et al.
Summary: Ion-exchanged ZSM-5 zeolites were prepared as bifunctional catalysts for the conversion of glucose to levulinic acid (LA). Microwave-assisted solid-state ion-exchange technique was used to obtain ZSM-5 catalysts with improved acidity. Among the metal ions used, Cu(II) showed the best performance.
BIOMASS CONVERSION AND BIOREFINERY
(2022)
Article
Energy & Fuels
Shuo Feng et al.
Summary: The study prepared a series of W-Zr-ZSM-5 (WZZ) catalysts using different preparation methods and found that the catalyst prepared by the sol-gel method (WZZ-SG700) exhibited the highest NO conversion and better performance. It also showed high resistance to SO2 and H2O and high N-2 selectivity.
Article
Chemistry, Physical
Ran Zhao et al.
Summary: This study investigated the catalytic performance and mechanisms of metal-doped M-CePO4 catalysts in NH3-SCR reaction, showing that metal doping improved the activity and stability of the catalyst, while providing more reaction sites.
MOLECULAR CATALYSIS
(2022)
Article
Energy & Fuels
Cheng Liu et al.
Summary: The elucidation of selective catalytic reduction mechanisms over metal-promoted zeolites is important for removing nitric oxides. In this study, copper/ZSM-5 showed the highest catalytic activity, while nickel/ZSM-5 exhibited weaker activity, with low-temperature peak induced by nickel clusters dispersed on the ZSM-5 surface. The results demonstrate the relationship between zeolite structure and catalyst properties for improving selective catalytic reduction.
CARBON RESOURCES CONVERSION
(2022)
Article
Engineering, Environmental
Tianle Ye et al.
Summary: The task of circular economy in mining industry is to develop and utilize a large number of tailing residue that has been shelved for a long time. An economical and sustainable utilization strategy of potassium feldspar tailing residue is reported. The ZSM-5 zeolite catalysts using tailing residue as raw materials by a template-free hydrothermal method are synthesized for selective catalytic reduction (SCR), abandoning the high pollution and energy consumption method of zeolite synthesis from fine chemicals. The effects of feed NaOH and Al-2(SO4)(3)center dot 18H(2)O on tailing residue and zeolite products are systematically studied, which proved that the silicon and aluminum elements in the tailing residue can be efficiently utilized. The results of scaling up experiment and experiment without additional aluminum confirm the feasibility and repeatability of tailing residue utilization. The synthesized ZSM-5 was used to prepare the Ce-Fe-ZSM-5 catalyst for NO reduction to N-2 and showed excellent activity, with the NOx conversion remaining above 80% at the range of 300 degrees C similar to 500 degrees C. The synergistic effect of Ce and Fe ions promoted the formation of more chemisorbed oxygen and accelerated the reaction rate of NO and NH3 adsorbed on the catalyst surface, resulting in a significant increase in the low-temperature activity of 1%Ce-Fe-ZSM-5. In this study, zeolite catalysts with excellent catalytic effect from tailing residue that can be used in petrochemical fields are successfully synthesized. The route is economic, environmental, and recyclable, which provides an opportunity for comprehensive development and application of tailing residue.
JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING
(2022)
Article
Chemistry, Physical
Gang Sun et al.
Summary: The NH3-SCR reactivity of Fe-AEI zeolite was improved by introducing Cu ions, leading to enhanced activity and hydrothermal stability. The optimized Cu/Fe-AEI bimetallic catalyst showed the best NO conversion in triplicate SO2 poisoning and regeneration tests.
CATALYSIS SCIENCE & TECHNOLOGY
(2022)
Article
Chemistry, Multidisciplinary
Hue-Tong Vu et al.
Summary: Catalyst design is crucial for improving catalytic activity and product selectivity. This study presents a systematic structural study of Ni in the Ni/ZSM-5 materials, revealing the changes in the local environment of Ni species induced by the different Al contents of the parent ZSM-5. The results show that the number of highly reducible and active NiO crystals is strongly correlated with the framework Al sites present in ZSM-5 zeolites, which is beneficial for further investigation of the catalytic activities of Ni/ZSM-5 and other metal-modified bifunctional catalysts.
NANOSCALE ADVANCES
(2022)
Article
Chemistry, Physical
Ziyi Chen et al.
Summary: Submonolayer-supported catalysts based on 3DOM CeO(2) loaded with VOx-MnOx exhibit excellent activity for NH3-SCR, with the 5 wt% 3DOM VOx-MnOx/CeO2 catalyst showing the best catalytic performance achieving over 95% NO conversion at 250 degrees C.
Article
Chemistry, Physical
Jiali Zhang et al.
Summary: CuO@TiO2 core-shell nanostructure catalyst showed significantly higher activity in NH3-SCR reaction, benefiting from better redox ability, more oxygen vacancies, acid sites, and NOx species on the catalyst. The reaction mechanism may involve both Eley-Rideal (E-R) and Langmuir-Hinshewood (L-H) mechanisms. These findings may contribute to the development of effective non-vanadium-based SCR catalysts.
Article
Chemistry, Multidisciplinary
Shunyu Han et al.
Summary: A one-step acid treatment method was developed for synthesizing hierarchical HZSM-5, while hierarchical Mg/ZSM-5 was obtained by the incipient impregnation method to increase propylene yield in the methanol-to-propylene reaction. The samples were characterized by various techniques, showing improved SiO2/Al2O3 molar ratio and well-distributed acid sites. The hierarchical Mg/ZSM-5 exhibited high propylene selectivity and resistance to carbon deposition in the MTP reaction.
RESEARCH ON CHEMICAL INTERMEDIATES
(2021)
Article
Chemistry, Physical
Jinkun Guan et al.
Summary: The Gd-modified MnOx/ZSM-5 catalysts showed excellent catalytic activity and SO2 resistance in low-temperature NH3-SCR reactions, attributed to their large surface area, abundant Mn4+ and surface oxygen species, strong reducibility, and suitable acidity. The addition of Gd inhibited the reaction between SO2 and MnOx active sites, leading to enhanced SO2 resistance. Furthermore, the mechanism of low-temperature SCR reactions over Mn/Z and GdMn/Z-0.3 was found to follow the Langmuir-Hinshelwood and Eley-Rideal mechanism, as revealed by in situ DRIFTS experiments.
Article
Chemistry, Physical
Tong Qiao et al.
Summary: The study demonstrates that the location of MnOx nanoparticles in MnOx-ZSM-5 catalysts significantly influences the catalytic activity for NH3-SCR, with MnOx clusters dispersed on the outside exhibiting higher activity at low temperatures than those encapsulated in the channels of the support. The redox ability and Mn3+ species play crucial roles in enhancing the oxidation of NO and formation of unstable NOx intermediates, ultimately improving the SCR activity at lower temperatures.
APPLIED CATALYSIS A-GENERAL
(2021)
Article
Chemistry, Multidisciplinary
Houda Jouini et al.
Summary: The addition of Ce affects the textural and structural properties of the Fe-Cu-MFI system, with Ce-promoted samples showing better NO conversion activity up to 450 degrees Celsius. The presence of Ce in aged catalysts also reduces the loss of activity.
RESEARCH ON CHEMICAL INTERMEDIATES
(2021)
Article
Chemistry, Physical
Vijay Khanal et al.
Summary: A wet chemical-synthesized high surface area ultrafine Ta2O5 nanoparticle and its application to NOx control was reported, showing better photocatalytic activity and stability compared to TiO2.
APPLIED CATALYSIS B-ENVIRONMENTAL
(2021)
Article
Chemistry, Physical
Hongyan Xue et al.
Summary: A series of MnCo/Cu-Z catalysts with different Mn/Co ratios were prepared and investigated for the SCR of NO with NH3. The Mn1Co2/Cu-Z catalyst showed the highest activity, with high-valent metal ion enrichment and improved metal oxide reducibility contributing to its enhanced catalytic performance. The nitrate species on the catalyst surface and SCR mechanism play crucial roles in the catalytic activity of MnCo/Cu-Z.
Article
Chemistry, Physical
Hongyan Xue et al.
Summary: The study established the poisoning effect of K on Cu/ZSM-5 in NH3-SCR through various characterization methods, revealing decreased exposure of active CuO, inhibited adsorption of NH3 and NOx, minimized formation of active bridged nitrate, and facilitated formation of inactive bidentate nitrate.
COLLOID AND INTERFACE SCIENCE COMMUNICATIONS
(2021)
Article
Chemistry, Inorganic & Nuclear
A. Manafi et al.
Summary: A novel method for manganese oxide deposition on clay-bonded SiC supports using AA-MOCVD technique was reported. The effects of deposition temperature on the physicochemical characteristics of the composite material were investigated, with a deposition temperature of 340 degrees C showing optimal catalytic behavior for propane-selective catalytic reduction of NOx.
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
(2021)
Review
Chemistry, Multidisciplinary
Guiying Xu et al.
Summary: This review discusses the importance of NOx removal, the effects of H2O and SO2 on catalysts, and the resistance of Mn-based catalysts. It analyzes the impact of factors such as metal modification and support selection on resistance, and proposes future research focus and countermeasures to solve existing problems.
Article
Environmental Sciences
Yuanyuan Ma et al.
ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH
(2020)
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Chemistry, Applied
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TOPICS IN CATALYSIS
(2020)
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CATALYSIS COMMUNICATIONS
(2020)
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APPLIED CATALYSIS A-GENERAL
(2020)
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APPLIED CATALYSIS A-GENERAL
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CHEMICAL ENGINEERING JOURNAL
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Xiaomin Wu et al.
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(2019)
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CATALYSIS SURVEYS FROM ASIA
(2019)
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Rob Jeremiah G. Nuguid et al.
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Xue-tao Wang et al.
ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH
(2019)
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INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH
(2019)
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Zhengcheng Wen et al.
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Hongyan Xue et al.
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M. Hamidzadeh et al.
INTERNATIONAL JOURNAL OF ENVIRONMENTAL SCIENCE AND TECHNOLOGY
(2018)
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M. Bendrich et al.
APPLIED CATALYSIS B-ENVIRONMENTAL
(2018)
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Yu Shen et al.
JOURNAL OF POROUS MATERIALS
(2018)
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Huazhen Chang et al.
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(2018)
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REACTION KINETICS MECHANISMS AND CATALYSIS
(2018)
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APPLIED PETROCHEMICAL RESEARCH
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Yanke Yu et al.
CATALYSIS SCIENCE & TECHNOLOGY
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CATALYSIS SCIENCE & TECHNOLOGY
(2016)
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TOPICS IN CATALYSIS
(2015)
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CHINESE JOURNAL OF CATALYSIS
(2015)
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Ferenc Lonyi et al.
APPLIED CATALYSIS B-ENVIRONMENTAL
(2014)
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JOURNAL OF CATALYSIS
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JOURNAL OF CATALYSIS
(2012)
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APPLIED CATALYSIS A-GENERAL
(2010)
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BI Kwak et al.
JOURNAL OF MATERIALS SCIENCE LETTERS
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