期刊
JOURNAL OF TESTING AND EVALUATION
卷 52, 期 1, 页码 534-544出版社
AMER SOC TESTING MATERIALS
DOI: 10.1520/JTE20230335
关键词
alumina; ceramics; density; outgassing; vacuum
This study systematically assesses the influence of internal structure on the outgassing property of alumina ceramics. The results show that denser alumina structure leads to lower outgassing rate, and the internal structure also has some influence on the outgassing characteristics of the material.
In order to systematically assess the influence of the internal structure on the outgassing property, alumina ceramics with different porosity were first prepared by four sintering processes, and then their measurements of the outgassing rate and desorption gas components were performed using the throughput method. Experimental results show that when the alumina sample is exposed to vacuum for just a few hours, surface outgassing dominants and the main outgassing component is water vapor. After sufficiently long vacuum extraction, the gas inside the alumina ceramic is gradually released. In this test, the gas released from the internal structure plays a dominant role after 48 h pumping of 600 L/s. Combined with the microstructure analysis, it is further concluded that the denser the alumina structure is, the lower the vacuum outgassing rate is and the lower the partial pressure of the individual gas components is. It can also be observed that the internal structure still has some influence on the outgassing characteristics of the material, although to a slightly lower degree than the surface properties compared to previous studies.
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