期刊
CHEMICAL COMMUNICATIONS
卷 51, 期 39, 页码 8349-8352出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5cc02386f
关键词
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Tertiary cyclopropanols react rapidly with Togni reagent in methanol at room temperature in the presence of catalytic amounts (3 mol%) of CuCl affording beta-trifluoromethyl ketones in 65-73% isolated yields. Ring opening in 1,2-dialkylsubstituted cyclopropanols gives a mixture of isomeric beta-trifluoromethyl ketones in about 50% combined yield.
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