Enhancements of critical current density in Bi1.6Pb0.4Sr2Ca2Cu3O10+δ superconductors by additions of SnO2 nanoparticles

The impact of adding SnO2 nanoparticles on the enhancements of critical current density (Jc) of the Bi1.6Pb0.4Sr2Ca2Cu3O10+& delta; superconductors was studied. Polycrystalline superconductors with stoichiometry of (Bi1.6Pb0.4Sr2Ca2Cu3O10+& delta;)1-x(SnO2)x where was x was ranged from 0.000, 0.002, 0.004, 0.006, 0.008 to 0.010 were made through traditional solid state reaction technique. X-ray diffraction data revealed that all fabricated samples consisted of Bi-2223 and Bi-2212 superconducting phases. The volume fraction of the Bi-2223 phase decreased with SnO2 addition. Analyses of textural structure using scanning electron microscopy data evidenced a clear decrease in grain orientation and porosity with increased doping levels. SnO2 presence in connection to Bi-2223 deceleration reduced the critical temperature. Values of Jc deduced from the magnetization hysteresis loops measured at different temperatures of 35 K, 45 K, 55 K, 65 K were found to enhance for the SnO2 added samples. In the x = 0.002 samples, the field dependent Jc achieved its maximum values. In order to have a deeper understanding in the improvements of flux pinning properties, small and large bundle fields were determined by using the collective pinning theory. The obtained values indicate the expansion of the two corresponding regimes with appropriate. By analyzing the dependence of normalized Jc versus normalized critical temperature, the dominant flux pinning mechanisms in all samples were consistent with & delta;l pinning. Besides, the addition of SnO2 nanoparticles was likely to produce pinning centers in form of core point as evidenced by using the Dew-Hughes model.

Automated summary

The study examined the effects of adding SnO2 nanoparticles on the enhancement of critical current density (Jc) in Bi1.6Pb0.4Sr2Ca2Cu3O10+& delta; superconductors. Polycrystalline superconductors with varying levels of SnO2 doping were prepared. X-ray diffraction analysis showed that all samples consisted of Bi-2223 and Bi-2212 superconducting phases, with a decrease in the volume fraction of the Bi-2223 phase with SnO2 addition. Scanning electron microscopy data revealed a decrease in grain orientation and porosity with increased SnO2 doping levels. The addition of SnO2 nanoparticles led to an increase in Jc values, with the maximum values achieved at x = 0.002.