☆ 4.8 Article

Development of Electrochemical Cells and Their Application for Spatially Resolved Analysis Using a Multitechnique Approach: From Conventional Experiments to X-Ray Nanoprobe Beamlines

ANALYTICAL CHEMISTRY (2023)

相关参考文献

注意：仅列出部分参考文献，下载原文获取全部文献信息。

Article Chemistry, Physical

Chemical Limits on X-ray Nanobeam Studies in Water

Alexander Bjorling et al.

Summary: Recently, there has been increasing interest in operando X-ray studies of chemical reactions, facilitated by the development of powerful focused X-ray sources. In this study, we demonstrate how an X-ray nanobeam induces a phase transition in shape-controlled Pd nanoparticles and propose a chemical reaction-diffusion model to explain the observations. The model also suggests that high concentrations of reactive species may arise under any focused X-ray probe, challenging the validity of these methods in aqueous chemical and catalytic systems.

JOURNAL OF PHYSICAL CHEMISTRY C (2023)

添加到收藏夹

Review Chemistry, Multidisciplinary

Beginner's Guide to Raman Spectroelectrochemistry for Electrocatalysis Study

Weiran Zheng

Summary: This article provides an essential experimental guideline of in situ Raman spectroelectrochemistry for beginners. After introducing the technical principle and primary applications, the article focuses on experimental considerations and highlights recent efforts to make the technique more affordable.

CHEMISTRYMETHODS (2023)

添加到收藏夹

Review Chemistry, Multidisciplinary

Microfluidics for Electrochemical Energy Conversion

Omar A. Ibrahim et al.

Summary: This review comprehensively synthesizes the best practices in the field of microfluidics for electrochemical energy conversion, including cell designs, fabrication techniques, and device functions. It assesses all research contributions and discusses emerging technologies and future research directions.

CHEMICAL REVIEWS (2022)

添加到收藏夹

Review Materials Science, Multidisciplinary

Entropy stabilized multicomponent oxides with diverse functionality - a review

Ashritha Salian et al.

Summary: High-entropy oxides (HEOs) have captured significant scientific attention for their exceptional and tunable properties, with the main driving force being the control of configurational entropy to achieve phase purity. These new oxide candidates show great potential for practical applications and represent a key frontier for researchers to explore.

CRITICAL REVIEWS IN SOLID STATE AND MATERIALS SCIENCES (2022)

添加到收藏夹

Article Chemistry, Analytical

Nanoscale Visualization of Electrochemical Activity at Indium Tin Oxide Electrodes

Oluwasegun J. Wahab et al.

Summary: This study investigates nanoscale electrochemistry at indium tin oxide (ITO) electrodes using high-resolution scanning electrochemical cell microscopy (SECCM). The research reveals the spatially heterogeneous charge transfer activity of ITO surfaces and measures a significantly higher charge transfer rate at the nanoscale compared to the macroscale.

ANALYTICAL CHEMISTRY (2022)

添加到收藏夹

Article Energy & Fuels

An Overview of Hydrogen Production: Current Status, Potential, and Challenges

Muhammad Younas et al.

Summary: Hydrogen as an energy carrier can provide a long term solution to sustainable and environmentally friendly fuel supply, but it must come from renewable sources to be truly considered a clean fuel. Electrolysis, contributing 4% of the world's energy demand, still faces challenges due to its high energy consumption. Plasmolysis has been suggested as a competitive alternative with lower power consumption and cost.

FUEL (2022)

添加到收藏夹

Article Chemistry, Multidisciplinary

Bragg coherent diffraction imaging of single 20 nm Pt particles at the ID01-EBS beamline of ESRF

M- Richard et al.

Summary: This study successfully measured the three-dimensional shape and strain of platinum nanoparticles with a diameter smaller than 30 nm using Bragg coherent diffraction imaging, opening up new possibilities for the observation of realistic catalytic particles.

JOURNAL OF APPLIED CRYSTALLOGRAPHY (2022)

添加到收藏夹

Article Chemistry, Physical

Role of Ni in PtNi Bimetallic Electrocatalysts for Hydrogen and Value-Added Chemicals Coproduction via Glycerol Electrooxidation

Hui Luo et al.

Summary: PtNi2 catalyst with a moderate Ni content and a homogenously alloyed structure exhibited the highest reaction activity in the electrochemical oxidation of glycerol among all materials studied. The role of Ni in PtNi is to tailor the electronic structure of pure Pt sites, influencing the glycerol oxidation reaction.

ACS CATALYSIS (2022)

添加到收藏夹

Article Chemistry, Physical

Learning from the Heterogeneity at Electrochemical Interfaces

C. Hyun Ryu et al.

Summary: Understanding the role of heterogeneity in electrochemistry is crucial for improving the performance of electrochemical devices. This Perspective discusses the importance of heterogeneity in electrochemical interfaces, explores current methods for revealing heterogeneity, and provides perspectives on utilizing heterogeneity to design more efficient electrochemical devices.

JOURNAL OF PHYSICAL CHEMISTRY LETTERS (2022)

添加到收藏夹

Article Chemistry, Physical

Bridging the Gap between Single Nanoparticle Imaging and Global Electrochemical Response by Correlative Microscopy Assisted By Machine Vision

Louis Godeffroy et al.

Summary: This study investigates the microscale behavior of electrochemical interfaces by utilizing various microscopy techniques. By automatically identifying the physical and chemical characteristics of nanoparticles, the researchers reconstructed the overall electrochemical response. The research reveals that the activity of nickel metal in the electrocatalysis of hydrogen evolution reaction is comparable to that of platinum.

SMALL METHODS (2022)

添加到收藏夹

Article Chemistry, Inorganic & Nuclear

Nanomaterials as electrocatalyst for hydrogen and oxygen evolution reaction: Exploitation of challenges and current progressions

Shujit Chandra Paul et al.

Summary: Electrocatalytic water splitting is seen as a promising sustainable source of renewable energy for the future. Challenges remain in developing cost-effective electrocatalysts with high surface area, stability, and bifunctional activity in order to overcome current barriers.

POLYHEDRON (2021)

添加到收藏夹

Article Multidisciplinary Sciences

Development of a sticker sealed microfluidic device for in situ analytical measurements using synchrotron radiation

Itamar T. Neckel et al.

Summary: Utilizing synchrotron light to explore microfluidic systems at the nanoscale can reveal new properties and functionalities of materials in various areas. The multifunctional polyester/glass microfluidic device presented in this work is chemically resistant and transparent to X-rays, suitable for both standard laboratory experiments and in situ analytical experiments across a wide electromagnetic window.

SCIENTIFIC REPORTS (2021)

添加到收藏夹

Review Chemistry, Multidisciplinary

Bragg Coherent Diffraction Imaging for In Situ Studies in Electrocatalysis

Rafael A. Vicente et al.

Summary: Electrocatalysis plays a crucial role in the present and future sustainable economy, with nanomaterials being of significant importance in this field. Bragg coherent diffraction imaging (BCDI) offers insights into the impact of lattice strain on electronic configuration and binding energy with reaction intermediates in nanomaterials. Despite challenges, BCDI has the potential to contribute to advancements in future electrocatalysis research.

ACS NANO (2021)

添加到收藏夹

Article Electrochemistry

Scanning Electrochemical Cell Microscopy in a Glovebox: Structure-Activity Correlations in the Early Stages of Solid-Electrolyte Interphase Formation on Graphite

Daniel Martin-Yerga et al.

Summary: This study uses scanning electrochemical cell microscopy (SECCM) to investigate the formation of solid-electrolyte interphase (SEI) on graphite surfaces in Li-ion batteries. The presence of step edges on the surface promotes the formation of a more passivating SEI. The study also shows that an unstable SEI can be detected under fast formation conditions, while a slow formation rate leads to the growth of an increasingly passivating SEI.

CHEMELECTROCHEM (2021)

添加到收藏夹

Article Multidisciplinary Sciences

Correlative operando microscopy of oxygen evolution electrocatalysts

J. Tyler Mefford et al.

Summary: Transition metal (oxy)hydroxides are promising electrocatalysts for the oxygen evolution reaction, with their properties evolving dynamically and heterogeneously with applied voltage. By studying single-crystalline beta-Co(OH)(2) platelet particles, researchers have found that the particles change structure and composition from inactive to active states as the voltage increases, ultimately linking bulk ion-insertion with surface catalytic activity. This study demonstrates the importance of understanding the nanoscale structure of electrocatalysts in predicting and optimizing their oxygen evolution activity.

NATURE (2021)

添加到收藏夹

Review Energy & Fuels

New roads and challenges for fuel cells in heavy-duty transportation

David A. Cullen et al.

Summary: The recent release of hydrogen economy roadmaps highlights the need for increased global investment in hydrogen production, storage, infrastructure and utilization. The shift in focus towards heavy-duty vehicle applications for fuel cell technologies is discussed, along with the required improvements in fuel cell systems and materials to meet efficiency and durability requirements. The article also summarizes the latest market outlooks and targets for heavy-duty vehicle applications.

NATURE ENERGY (2021)

添加到收藏夹

Article Chemistry, Multidisciplinary

From NiMoO4 to γ-NiOOH: Detecting the Active Catalyst Phase by Time Resolved in Situ and Operando Raman Spectroscopy

Robin N. Durr et al.

Summary: This study investigates NiMoO4 as a catalyst for the oxygen evolution reaction, showing its phase transformation under applied bias and the leaching of molybdenum from the catalyst. Molybdenum leaching increases the number of active sites on the catalyst, leading to higher current densities. Different NiMoO4 nanostructures influence the stability of the catalyst in alkaline media.

ACS NANO (2021)

添加到收藏夹

Review Chemistry, Multidisciplinary

What Makes High-Entropy Alloys Exceptional Electrocatalysts?

Tobias Loeffler et al.

Summary: By discussing the existing fundamental knowledge, researchers explore new concepts in catalyst design with the formation of multiple active sites in compositionally complex solid solution materials, commonly known as high-entropy alloys. The study critically assesses the opportunities and limitations of this material class while proposing a roadmap for potential breakthroughs in (electro)catalysis research.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2021)

添加到收藏夹

Review Chemistry, Multidisciplinary

Semiconducting Nanoparticles: Single Entity Electrochemistry and Photoelectrochemistry

S. Mathuri et al.

Summary: Semiconducting nanoparticles are crucial for emerging technological applications such as optoelectronic devices, sensors, and catalysts. Recent research on single entity electrochemistry and photoelectrochemistry of SC NPs through nano-impact method has gained increasing interest. This field enables the discoveries of intrinsic (photo) electrochemical activities of SC NPs at the single particle level.

FRONTIERS IN CHEMISTRY (2021)

添加到收藏夹

Article Chemistry, Physical

Electrochemical synthesis of multimetallic nanoparticles and their application in alkaline oxygen reduction catalysis

Joon Ho Park et al.

APPLIED SURFACE SCIENCE (2020)

添加到收藏夹

Review Chemistry, Physical

Promises of Main Group Metal-Based Nanostructured Materials for Electrochemical CO2 Reduction to Formate

Na Han et al.

ADVANCED ENERGY MATERIALS (2020)

添加到收藏夹

Editorial Material Chemistry, Multidisciplinary

Electrocatalysis: A Core Technique for a Sustainable Future

Zhichuan J. Xu et al.

CHEMISTRY-A EUROPEAN JOURNAL (2020)

添加到收藏夹

Article Chemistry, Multidisciplinary

Super-Resolution Infrared Imaging of Polymorphic Amyloid Aggregates Directly in Neurons

Oxana Klementieva et al.

ADVANCED SCIENCE (2020)

添加到收藏夹

Article Chemistry, Physical

In Situ/Operando Studies for Designing Next-Generation Electrocatalysts

Yanping Zhu et al.

ACS ENERGY LETTERS (2020)

添加到收藏夹

Review Chemistry, Multidisciplinary

Electrocatalysis as the Nexus for Sustainable Renewable Energy: The Gordian Knot of Activity, Stability, and Selectivity

Justus Masa et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2020)

添加到收藏夹

Review Chemistry, Physical

Scanning electrochemical cell microscopy: A natural technique for single entity electrochemistry

Oluwasegun J. Wahab et al.

CURRENT OPINION IN ELECTROCHEMISTRY (2020)

添加到收藏夹

Review Chemistry, Physical

Recent developments in catalyst -related PEM fuel cell durability

Rodney L. Borup et al.

CURRENT OPINION IN ELECTROCHEMISTRY (2020)

添加到收藏夹

Article Chemistry, Physical

Electrooxidation of C4 Polyols on Platinum Single-Crystals: A Computational and Electrochemical Study

Gabriela Soffiati et al.

JOURNAL OF PHYSICAL CHEMISTRY C (2020)

添加到收藏夹

Article Chemistry, Multidisciplinary

PyNX: high-performance computing toolkit for coherent X-ray imaging based on operators

Vincent Favre-Nicolin et al.

JOURNAL OF APPLIED CRYSTALLOGRAPHY (2020)

添加到收藏夹

Article Physics, Multidisciplinary

Three-Dimensional Coherent Bragg Imaging of Rotating Nanoparticles

Alexander Bjorling et al.

PHYSICAL REVIEW LETTERS (2020)

添加到收藏夹

Article Chemistry, Multidisciplinary

Water oxidation intermediates on iridium oxide electrodes probed by in situ electrochemical SHINERS

Khezar H. Saeed et al.

CHEMICAL COMMUNICATIONS (2020)

添加到收藏夹

Review Chemistry, Multidisciplinary

Paired electrolysis for simultaneous generation of synthetic fuels and chemicals

Natalia P. Martinez et al.

NEW JOURNAL OF CHEMISTRY (2020)

添加到收藏夹

Article Chemistry, Physical

Bi-modified Pt Electrodes toward Glycerol Electrooxidation in Alkaline Solution: Effects on Activity and Selectivity

Matheus B. C. de Souza et al.

ACS CATALYSIS (2019)

添加到收藏夹

Article Instruments & Instrumentation

The Nanodiffraction beamline ID01/ESRF: a microscope for imaging strain and structure

Steven J. Leake et al.

JOURNAL OF SYNCHROTRON RADIATION (2019)

添加到收藏夹

Article Chemistry, Analytical

Single Nanoparticle Electrochemistry

Fato Tano Patrice et al.

ANNUAL REVIEW OF ANALYTICAL CHEMISTRY, VOL 12 (2019)

添加到收藏夹

Article Nanoscience & Nanotechnology

Unraveling the Role of Sn Segregation in the Electronic Transport of Polycrystalline Hematite: Raising the Electronic Conductivity by Lowering the Grain-Boundary Blocking Effect

Mario R. S. Soares et al.

ADVANCED ELECTRONIC MATERIALS (2019)

添加到收藏夹

Article Chemistry, Physical

Identification of FeN4 as an Efficient Active Site for Electrochemical N2 Reduction

Chao He et al.

ACS CATALYSIS (2019)

添加到收藏夹

Review Chemistry, Physical

Glycerol Electro-Oxidation in Alkaline Media and Alkaline Direct Glycerol Fuel Cells

Ermete Antolini

CATALYSTS (2019)

添加到收藏夹

Article Electrochemistry

Alumina contamination through polishing and its effect on hydrogen evolution on gold electrodes

Mariana C. O. Monteiro et al.

ELECTROCHIMICA ACTA (2019)

添加到收藏夹

Review Chemistry, Multidisciplinary

Nanoscale Surface Structure-Activity in Electrochemistry and Electrocatalysis

Cameron L. Bentley et al.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2019)

添加到收藏夹

Article Chemistry, Multidisciplinary

Local Surface Modifications Investigated by Combining Scanning Electrochemical Microscopy and Surface-Enhanced Raman Scattering

Jan Clausmeyer et al.

CHEMPLUSCHEM (2018)

添加到收藏夹

Article Materials Science, Multidisciplinary

The Coherent X-ray Sub-micro and Nanoprobe Stations for the CARNAUBA Beamline at the Sirius-LNLS Storage Ring.

Carlos A. Perez et al.

MICROSCOPY AND MICROANALYSIS (2018)

添加到收藏夹

Review Chemistry, Multidisciplinary

Perspective and Prospectus on Single-Entity Electrochemistry

Lane A. Baker

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2018)

添加到收藏夹

Article Chemistry, Analytical

Understanding CO oxidation reaction on platinum nanoparticles

Rosa M. Aran-Ais et al.

JOURNAL OF ELECTROANALYTICAL CHEMISTRY (2017)

添加到收藏夹

Article Chemistry, Physical

Simultaneous optical and electrochemical recording of single nanoparticle electrochemistry

Linlin Sun et al.

NANO RESEARCH (2017)

添加到收藏夹

Article Chemistry, Multidisciplinary

Why conclusions from platinum model surfaces do not necessarily lead to enhanced nanoparticle catalysts for the oxygen reduction reaction

Federico Calle-Vallejo et al.

CHEMICAL SCIENCE (2017)

添加到收藏夹

Article Chemistry, Physical

Emerging tools for studying single entity electrochemistry

Yixian Wang et al.

FARADAY DISCUSSIONS (2016)

添加到收藏夹

Article Chemistry, Physical

Emerging tools for studying single entity electrochemistry

Yixian Wang et al.

FARADAY DISCUSSIONS (2016)

添加到收藏夹

Article Energy & Fuels

Electrochemical conversion of alcohols for hydrogen production: a short overview

Christophe Coutanceau et al.

WILEY INTERDISCIPLINARY REVIEWS-ENERGY AND ENVIRONMENT (2016)

添加到收藏夹

Article Multidisciplinary Sciences

Finding optimal surface sites on heterogeneous catalysts by counting nearest neighbors

Federico Calle-Vallejo et al.

SCIENCE (2015)

添加到收藏夹

Review Chemistry, Multidisciplinary

Preparation and catalytic applications of nanomaterials: a review

Navneet Sharma et al.

RSC ADVANCES (2015)

添加到收藏夹

Review Chemistry, Analytical

Techniques and methodologies in modern electrocatalysis: evaluation of activity, selectivity and stability of catalytic materials

Aliaksandr S. Bandarenka et al.

ANALYST (2014)

添加到收藏夹

Review Chemistry, Physical

Approaches to Single-Nanoparticle Catalysis

Justin B. Sambur et al.

ANNUAL REVIEW OF PHYSICAL CHEMISTRY, VOL 65 (2014)

添加到收藏夹

Article Chemistry, Multidisciplinary

A Student-Made Silver-Silver Chloride Reference Electrode for the General Chemistry Laboratory: ∼10 min Preparation

Rebecca Barlag et al.

JOURNAL OF CHEMICAL EDUCATION (2014)

添加到收藏夹

Review Chemistry, Multidisciplinary

Shape-Controlled Synthesis of Pd Nanocrystals and Their Catalytic Applications

Hui Zhang et al.

ACCOUNTS OF CHEMICAL RESEARCH (2013)

添加到收藏夹

Review Chemistry, Multidisciplinary

Particle Size and Support Effects in Electrocatalysis

Brian E. Hayden

ACCOUNTS OF CHEMICAL RESEARCH (2013)

添加到收藏夹

Review Chemistry, Multidisciplinary

Shape-Control and Electrocatalytic Activity-Enhancement of Pt-Based Bimetallic Nanocrystals

Nathan S. Porter et al.

ACCOUNTS OF CHEMICAL RESEARCH (2013)

添加到收藏夹

Review Chemistry, Multidisciplinary

Nanostructured materials for applications in heterogeneous catalysis

Francisco Zaera

CHEMICAL SOCIETY REVIEWS (2013)

添加到收藏夹

Article Chemistry, Multidisciplinary

Pseudo-Single-Crystal Electrochemistry on Polycrystalline Electrodes: Visualizing Activity at Grains and Grain Boundaries on Platinum for the Fe2+/Fe3+ Redox Reaction

Barak D. B. Aaronson et al.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2013)

添加到收藏夹

Article Biochemical Research Methods

Microfluidic devices for X-ray studies on hydrated cells

Britta Weinhausen et al.

LAB ON A CHIP (2013)

添加到收藏夹

Review Chemistry, Multidisciplinary

Nanomaterials for renewable energy production and storage

Xiaobo Chen et al.

CHEMICAL SOCIETY REVIEWS (2012)

添加到收藏夹

Review Optics

A matter of scale: from far-field microscopy to near-field nanoscopy

Diedrich A. Schmidt et al.

LASER & PHOTONICS REVIEWS (2012)

添加到收藏夹

Review Electrochemistry

Thirty years of platinum single crystal electrochemistry

V. Climent et al.

JOURNAL OF SOLID STATE ELECTROCHEMISTRY (2011)

添加到收藏夹

Article Chemistry, Physical

Spectroscopic Studies of the Glycerol Electro-Oxidation on Polycrystalline Au and Pt Surfaces in Acidic and Alkaline Media

Janaina Fernandes Gomes et al.

ELECTROCATALYSIS (2011)

添加到收藏夹

Article Chemistry, Analytical

CO electrooxidation on carbon supported platinum nanoparticles: Effect of aggregation

Ana Lopez-Cudero et al.

JOURNAL OF ELECTROANALYTICAL CHEMISTRY (2010)

添加到收藏夹

Review Chemistry, Analytical

In situ structural characterization of electrochemical systems using synchrotron-radiation techniques

Roland De Marco et al.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2010)

添加到收藏夹

Review Chemistry, Analytical

Scanning Electrochemical Microscopy

Shigeru Amemiya et al.

ANNUAL REVIEW OF ANALYTICAL CHEMISTRY (2008)

添加到收藏夹

Article Chemistry, Physical

Size-dependent activity of gold nanoparticles for oxygen electroreduction in alkaline electrolyte

Wei Tang et al.

JOURNAL OF PHYSICAL CHEMISTRY C (2008)

添加到收藏夹

Article Nanoscience & Nanotechnology

Does nanoparticle activity depend upon size and crystal phase?

Jingkun Jiang et al.

NANOTOXICOLOGY (2008)

添加到收藏夹

Article Chemistry, Physical

Shape-dependent electrocatalysis: methanol and formic acid electrooxidation on preferentially oriented Pt nanoparticles

J. Solla-Gullon et al.

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2008)

添加到收藏夹

Article Chemistry, Physical

Surface characterization of platinum electrodes

Jose Solla-Gullon et al.

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2008)

添加到收藏夹

Article Chemistry, Multidisciplinary

Platinum nanoparticle shape effects on benzene hydrogenation selectivity

Kaitlin M. Bratlie et al.

NANO LETTERS (2007)

添加到收藏夹

Article Chemistry, Physical

Influence of particle agglomeration on the catalytic activity of carbon-supported Pt nanoparticles in CO monolayer oxidation

F Maillard et al.

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2005)

添加到收藏夹

Article Electrochemistry

Surface-oxide growth at platinum electrodes in aqueous H2SO4 Reexamination of its mechanism through combined cyclic-voltammetry, electrochemical quartz-crystal nanobalance, and Auger electron spectroscopy measurements

G Jerkiewicz et al.

ELECTROCHIMICA ACTA (2004)

添加到收藏夹

Article Chemistry, Multidisciplinary

Shape-dependent catalytic activity of platinum nanoparticles in colloidal solution

R Narayanan et al.

NANO LETTERS (2004)

添加到收藏夹

Letter Chemistry, Physical

Adsorbate interactions and phase transitions at the stepped platinum/electrolyte interface: experiment compared with Monte Carlo simulations

MTM Koper et al.

SURFACE SCIENCE (2001)

添加到收藏夹

© Peeref 2019-2024. All rights reserved.