☆ 4.8 Review

Electronic Structures and Photoredox Chemistry of Tungsten(0) Arylisocyanides

ACCOUNTS OF CHEMICAL RESEARCH (2023)

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Summary: In this study, four new copper(I) coordination complexes were synthesized and characterized. These complexes exhibit longer excited-state lifetimes and high photoluminescence quantum efficiencies. By adjusting the 2,9-substituents, the photophysical properties of these complexes can be tailored, providing new directions for the discovery of MLCT chromophores.

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Summary: This study presents a luminescent iron compound that exhibits dual emission behavior from ligand-to-metal charge transfer (LMCT)- and metal-to-ligand charge transfer (MLCT)-dominated states. The compound has a unique ligand design that enables the presence of energetically accessible MLCT states, providing potential for electron transfer reactions in photoredox catalysis.

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Summary: Photoredox catalysis has transformed synthetic chemistry and researchers have been exploring the use of low-energy deep red (DR) or near-infrared (NIR) light to overcome the limitations of high-energy blue/ultraviolet light. This graphical review summarizes the photophysical principles relevant to photoredox catalysis and reviews applications that benefit from low-energy irradiation, including large-scale batch reactions, photodynamic therapy, biological labeling, and multi-photon excitation.

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Summary: The photochemical cyclization of 1-(2-iodobenzyl)-pyrrole (IBP) and 1-(2-bromobenzyl)-pyrrole (BBP) to 5H-pyrrolo[2,1-a]isoindol catalyzed by W(CNDipp)6 was studied. The results showed that W(CNDipp)6 could effectively catalyze the cyclization of IBP, and this reaction was not inhibited by the addition of other reagents.

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Summary: Unlike platinum group metals, cobalt(III) complexes with mixed metal-to-ligand and intra-ligand charge transfer properties in the excited state have not been discovered yet. A stable cobalt(III) complex with substantial mixed metal-to-ligand and intra-ligand charge transfer character in the excited state was obtained by using a rigid tridentate chelate ligand.

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Javier Fajardo et al.

Summary: Homoleptic tungsten(0) arylisocyanides exhibit photophysical and photochemical properties comparable to archetypal ruthenium(II) and iridium(III) polypyridine complexes. By systematically varying the arylisocyanide ligands, it is possible to modulate the photophysical properties of these complexes while maintaining high optical performance.

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