期刊
CHEMICAL COMMUNICATIONS
卷 51, 期 53, 页码 10714-10717出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5cc03429a
关键词
-
资金
- National Natural Science Foundation of China [21173032, 21372035]
Two-step one-pot transformation of primary halides into corresponding nitriles is successfully achieved. Nucleophilic substitution of primary halides with sodium azide and subsequent palladium-catalyzed hydrogen transfer proceeds smoothly in the presence of sterically bulky ligand dicyclohexyl(2',4',6'-triisopropylbiphenyl-2-yl)phosphine (XPhos) in acetone to produce nitriles in satisfactory to good yields.
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