Mechanistic behaviour and modelling of creep in powder metallurgy FGH96 nickel superalloy

The creep properties of a nickel-based superalloy at 700 degrees C and 690 MPa resulting from differing aging heat treatments have been investigated. The heat treatments gave rise to significantly different tertiary gamma' precipitate distributions which in turn influence the propensity for precipitate shearing. The creep life was found to decrease with an increase of volume fraction of tertiary gamma'. It is shown that the gamma' precipitates undergo shearing by matrix dislocations resulting in residual stacking faults which have been identified from TEM studies. A physically-based crystal slip model for creep deformation in FGH96 has been developed. A critical gamma' precipitate size is found to exist above which precipitate shearing occurs by strongly-coupled dislocations pairs. The critical size for FGH96 superalloy is less than 15 nm, which is smaller than most of the gamma' precipitates in the aged treated samples. A bimodal precipitate hardening model has been presented from which the slip strength resulting from differing heat treatments may be determined. Creep strain rate is found to decrease with increasing slip strength. The crystal slip model successfully captures the effect of heat treatment (in terms of gamma' precipitate distributions) on resulting creep behaviour in alloy FGH96. (C) 2016 Elsevier B.V. All rights reserved.