☆ 4.4 Review

Recent Advancements in the Treatment of Emerging Contaminants Using Activated Persulfate Oxidation Process

SEPARATIONS (2023)

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Engineering carbon nanocatalysts towards efficient degradation of emerging organic contaminants via persulfate activation: A review

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Summary: This article provides a comprehensive review of the engineering of carbon nanocatalysts for the persulfate activated elimination of emerging organic contaminants (EOCs). The review highlights the advantages of carbon nanocatalysts, such as high stability and low toxicity, compared to metal-based counterparts. Current trends, applications, challenges, and future perspectives in this area are discussed, emphasizing the need for interdisciplinary collaborations.

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Electro-enhanced degradation of atrazine via Co-Fe oxide modified graphite felt composite cathode for persulfate activation

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Summary: In this study, a modified composite anode achieved efficient PS activation for atrazine degradation. Possible degradation pathways were proposed, providing a feasible strategy for enhancing the degradation of persistent organic pollutants.

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Synergistically enhanced activation of persulfate for efficient oxidation of organic contaminants using a microscale zero-valent aluminum/Fe-bearing clay composite

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Summary: Sulfate radical-based advanced oxidation processes have gained attention in contaminated water treatment. Microscale zero-valent aluminum (mZVAl) is an excellent electron donor and can activate persulfate (PS). However, the natural oxide layer of mZVAl hinders electron transfer. In this study, a composite material consisting of mZVAl and Fe-bearing clay (mZVAl-NaNAu-2) was obtained through ball milling and showed excellent efficiency in degrading various organic contaminants in water.

CHEMICAL ENGINEERING JOURNAL (2022)

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Hydrodynamic cavitation-enhanced heterogeneous activation of persulfate for tetracycline degradation: Synergistic effects, degradation mechanism and pathways

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Summary: This study proposes using hydrodynamic cavitation (HC) to enhance mass transfer and oxidant utilization in zero-valent iron (Fe-0) activated persulfate (PS) system. The results show that HC increases the reactivity of Fe-0 and improves the activation of PS. It is also found that the degradation of pollutants is more effective in acidic conditions. The mechanism of catalyst regeneration by HC is investigated using SEM, TEM, and BET analysis. This study provides valuable insights into the application of sulfate radical (SO4 center dot-) based advanced oxidation technologies (AOTs) in wastewater treatment.

CHEMICAL ENGINEERING JOURNAL (2022)

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Article Engineering, Chemical

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Metal-organic frameworks-derived catalysts for contaminant degradation in persulfate-based advanced oxidation processes

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Heterogeneous Photocatalytic Activation of Persulfate for the Removal of Organic Contaminants in Water: A Critical Review

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Summary: This review comprehensively discusses the fundamental understanding and rational design of heterogeneous photocatalytic persulfate-based advanced oxidation processes (AOPs). The review addresses the challenges and improvement strategies of these processes, and provides an overview of different types of heterogeneous photocatalytic persulfate-based AOPs. The review concludes by discussing the engineering implications and prospects for developing efficient and environmentally friendly AOPs for water treatment.

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Factorial design and optimization of thermal activation of persulfate for stabilized leachate treatment

Yun Tong Chin et al.

Summary: This study aims to investigate and compare the performance of thermally activated persulfate in treating stabilized leachate. By optimizing experimental operational factors such as S2O82-/COD ratio, temperature, and reaction time, it was found that the efficiency of persulfate oxidation for COD and colour removal significantly improved after thermal activation.

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A dandelion-like NiCo2O4 microsphere with superior catalytic activity as the mediator of persulfate activation for high-efficiency degradation of emerging contaminants

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Summary: A novel dandelion-like NiCo2O4 microsphere was synthesized and used as a catalyst for rapid degradation of organic pollutants, showing high catalytic activity and structural stability; The oxidation system demonstrated strong degradation capability towards various contaminants with low-toxicity byproducts; Redox couples of Co3+/Co2+ and Ni3+/Ni2+ were identified as main catalytic sites, with SO4· and · OH as main active species in the reaction system.

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Recent advances in persulfate-assisted TiO2-based photocatalysis for wastewater treatment: Performances, mechanism and perspectives

Ming Ge et al.

Summary: The use of persulfate-assisted TiO2 photocatalysis for wastewater treatment is an effective method to enhance the separation of electron/hole pairs and generate sulfate radicals for improved degradation of organic pollutants. Different modifications of TiO2 with carbon materials, transition metal-based catalysts, noble metals, and organic semiconductors have been explored to broaden its absorption spectrum and enhance charge separation, leading to increased efficiency in persulfate activation and pollutant degradation. Overall, the study also highlighted the importance of catalyst reusability and key operational parameters on the process efficiency, as well as proposed potential applications of persulfate-assisted TiO2 photocatalysis in water treatment.

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Pyrite-activated persulfate for simultaneous 2,4-DCP oxidation and Cr(VI) reduction

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Summary: Organic pollutants and heavy metals in wastewater were effectively removed simultaneously using pyrite and persulfate system, where SO4 center dot- and (OH)-O-center dot radicals were identified as the oxidative species responsible for degrading 2,4-DCP. Pyrite acted as a catalyst for Cr(VI) reduction, with Fe identified as the main catalytic site, showcasing a new strategy for the simultaneous removal of heavy metals and organic compounds in wastewater treatment.

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Iron-based persulfate activation process for environmental decontamination in water and soil

Ansaf Karim et al.

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Peracids - New oxidants in advanced oxidation processes: The use of peracetic acid, peroxymonosulfate, and persulfate salts in the removal of organic micropollutants of emerging concern - A review

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Intensified degradation of Acid Violet 7 dye using ultrasound combined with hydrogen peroxide, Fenton, and persulfate

Satyanarayana Kodavatiganti et al.

Summary: The study investigated the sonochemical degradation of acid Violet-7 dye using an ultrasonic bath. Results showed that lower dye concentration, acidic conditions, and lower temperature favored decolorization using only ultrasound, while combining ultrasound with Fenton's reagent resulted in almost 100% decolorization and 80.9% COD reduction.

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Central composite modeling for electrochemical degradation of paint manufacturing plant wastewater: One-step/two-response optimization

Dilara Ozturk et al.

Summary: Treatment of paint manufacturing wastewaters is a complex process, and electrochemical degradation can effectively remove color and COD, reducing energy consumption and operating costs.

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Nadeem A. Khan et al.

Summary: Industrial and hospital effluents, with high concentrations of pharmaceutical residues, pose challenges to traditional wastewater treatment plants. Biological treatment, while environmentally friendly, is less efficient at removing pharmaceutical residues compared to WWTP. Advanced oxidation processes like Fenton have shown promise, but high energy consumption hinders large-scale deployment. Integrated treatments combining Fenton with biological processes have been proposed as a solution for complete degradation of pharmaceutical residues in wastewater.

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Summary: This study found that PS was effective in degrading IBP under the influence of ultrasonic irradiation and mechanical mixing. Increasing PS concentration, rpm, and decreasing pH all led to higher IBP oxidation rates. The US/M-PS system showed promise as a method for treating IBP-based water pollutants.

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Remediation of real soil polluted with hexachlorocyclohexanes (α-HCH and β-HCH) using combined thermal and alkaline activation of persulfate: Optimization of the operating conditions

Alicia Checa-Fernandez et al.

Summary: The alkaline activation of persulfate (PS) intensified by temperature showed high efficiency in remediation of surface sediments contaminated with HCH-wastes. Under optimal conditions, complete conversion of alpha-HCH and 81% conversion of beta-HCH, with a dechlorination degree of 94%, were achieved in just 3 days.

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A meta-analysis of the scientific literature on (photo) Fenton and persulfate advanced oxidation processes: Where do we stand and where are we heading to?

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Minisci aroylation of N-heterocycles using choline persulfate in water under mild conditions

Joydev K. Laha et al.

Summary: The research aimed to develop persulfate mediated oxidative transformations that can be conducted at nearly room temperature using water as a solvent, eliminating the drawbacks of using organic solvents and higher temperatures in conventional metal persulfate reactions. This was achieved by utilizing choline persulfate for the reaction, demonstrating the Minisci reaction at 40 degrees C in water as the only solvent, and activating persulfate in an unconventional manner.

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Chongqing Wang et al.

Summary: This study systematically summarizes the research advances on PS activation by biochar-based materials in PS-AOPs, including modifications, characterizations, radical determinations, and catalytic mechanism. It introduces biochar modifications, characterization techniques, and catalytic mechanisms in PS-AOPs, offering novel insights into catalyst design and better understanding of PS-AOPs.

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K2S2O8 activation by glucose at room temperature for the synthesis and functionalization of heterocycles in water

Joydev K. Laha et al.

Summary: By utilizing the inexpensive oxidant K2S2O8 in water at room temperature, a sustainable and broad method for mild functionalization and synthesis of heterocycles has been demonstrated, avoiding the use of higher temperature, UV light, transition metals or bases typically required in traditional methods for persulfate activation.

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Survey of sono-activated persulfate process for treatment of real dairy wastewater

Hossein A. Panahi et al.

INTERNATIONAL JOURNAL OF ENVIRONMENTAL SCIENCE AND TECHNOLOGY (2020)

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Article Multidisciplinary Sciences

Rapid Removal of Tetrabromobisphenol A by Ozonation in Water: Oxidation Products, Reaction Pathways and Toxicity Assessment

Ruijuan Qu et al.

PLOS ONE (2015)

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Article Engineering, Environmental

Removal of 2-MIB and geosmin using UV/persulfate: Contributions of hydroxyl and sulfate radicals

Pengchao Xie et al.

WATER RESEARCH (2015)

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Article Engineering, Chemical

Kinetic oxidation of antipyrine in heat-activated persulfate

Chaoqun Tan et al.

DESALINATION AND WATER TREATMENT (2015)

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Article Engineering, Chemical

Heat-activated persulfate oxidation of sulfamethoxazole in water

Yu-qiong Gao et al.

DESALINATION AND WATER TREATMENT (2015)

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Article Engineering, Environmental

Degradation of chloramphenicol by thermally activated persulfate in aqueous solution

Minghua Nie et al.

CHEMICAL ENGINEERING JOURNAL (2014)

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Article Acoustics

Removal of 1,1,1-trichloroethane from aqueous solution by a sono-activated persulfate process

Bingzhi Li et al.

ULTRASONICS SONOCHEMISTRY (2013)

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Article Engineering, Environmental

Activated carbon catalyzed persulfate oxidation of Azo dye acid orange 7 at ambient temperature

Shiying Yang et al.

JOURNAL OF HAZARDOUS MATERIALS (2011)

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Article Engineering, Environmental

Persulfate Persistence under Thermal Activation Conditions

Richard L. Johnson et al.

ENVIRONMENTAL SCIENCE & TECHNOLOGY (2008)

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Review Chemistry, Physical

On the photolysis of simple anions and neutral molecules as sources of O-/OH, SOx- and Cl in aqueous solution

Hartmut Herrmann

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2007)

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