4.4 Article

Development of Bi2O3/MoSe2 mixed nanostructures for photocatalytic degradation of methylene blue dye

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TAYLOR & FRANCIS LTD
DOI: 10.1080/16583655.2022.2161333

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Mixed oxide nanocomposites; hydrothermal synthesis; degradation effeciency; methylene blue dye; photocatalyst

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Here, we demonstrate the sample and low-cost hydrothermal synthesis of a nanocomposite of Bi2O3/MoSe2 for hybrid photocatalyst. The structure of the synthesized samples was characterized using various techniques, and the Bi2O3/MoSe2 nanocomposite showed enhanced photocatalytic activity due to its high crystallinity, surface area, and small particle size. The results indicate that the Bi2O3/MoSe2 sample exhibited the highest photocatalytic degradation efficiency for the disintegration of methylene blue under visible illumination.
Herein, we demonstrate the sample and low coast hydrothermal synthesis of a nanocomposite of Bi2O3/MoSe2 for hybrid photocatalyst. The structure of as-synthesized samples was characterized by using several techniques, including XRD spectroscopy, Raman spectroscopy, XPS, SEM, BET, and UV-visible absorption spectroscopy. The nitrogen adsorption-desorption measurements show that the samples have a mesoporous texture with slits like pores. The Bi2O3/MoSe2 nanocomposite had BET surface areas of 36.439 m(2)/g, which were more than those of Bi2O3 (18.342 m(2)/g) and MoSe2 (12.923 m(2)/g). Under visible illumination, the photocatalytic activities of pure samples ( Bi2O3 and MoSe2) and the hybrid Bi2O3/MoSe2 sample for the disintegration of methylene blue were assessed. The results show that the Bi2O3/MoSe2 sample showed the highest photocatalytic degradation efficiency (i.e. 96.5% after an exposure time of 80 min). The increased photocatalytic activity is due to the mixed sample's high crystallinity and surface area, as well as the small particle size.

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