期刊
JOURNAL OF WOOD CHEMISTRY AND TECHNOLOGY
卷 36, 期 4, 页码 259-269出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/02773813.2015.1137945
关键词
Acid hydrolysis lignin; oxidation; NMR; MALDI-MS; MS(ESI)
资金
- Russian Science Foundation [14-13-00448]
Products of oxidation of industrial acid hydrolysis lignin in the H2O2-H2SO4 system were studied using C-13 NMR (in solution and solid state), MALDI-MS, and MS(ESI) techniques. Oxidation of hydrolysis lignin leads to the opening of aromatic rings of lignin, yielding carboxylic groups. Alkyl aryl ether linkages (beta-O-4-bonds) between lignin phenyl propane units are not significantly affected by the oxidation. The structure of oxidized hydrolysis lignin is proposed. The basic structural unit of oxidized hydrolysis lignin is a muconic acid derivative.
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