Raman spectroscopy of carbon materials and their composites: Graphene, nanotubes and fibres

Article Chemistry, Physical

Data cluster analysis and machine learning for classification of twisted bilayer graphene

Tom Vincent et al.

Summary: This study combines Raman spectroscopy with Gaussian mixture model to identify specific twist angle regions in twisted bilayer graphene, enabling high-throughput fabrication of TBLG.

CARBON (2023)

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Article Nanoscience & Nanotechnology

Deformation of and Interfacial Stress Transfer in Ti3C2 MXene-Polymer Composites

Mufeng Liu et al.

Summary: Research findings demonstrate that Ti3C2Tx MXene is an effective mechanical reinforcement material in polymer matrices, with mechanical properties less dependent on flake thickness compared to graphene. MXene's active surface chemistry enables possible functionalization for stronger interface with polymers, making it suitable for applications in strain engineering, mechanical enhancement, and materials such as membranes, coatings, and textiles.

ACS APPLIED MATERIALS & INTERFACES (2022)

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Article Materials Science, Composites

Mechanisms of reinforcement of PVA-Based nanocomposites by hBN nanosheets

Weimiao Wang et al.

Summary: A systematic study was conducted on the reinforcement of PVA by hBN nanosheets produced by liquid-phase exfoliation, revealing that BNNSs with larger aspect ratio exhibit the highest level of reinforcement, although a decline was observed at the highest loadings. Raman spectroscopy can be used to evaluate the distribution of BNNSs in nanocomposites and monitor stress transfer to BNNSs from the polymer matrix.

COMPOSITES SCIENCE AND TECHNOLOGY (2022)

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Article Materials Science, Multidisciplinary

Silane-functionalized graphene nanoplatelets for silicone rubber nanocomposites

He Ren et al.

Summary: The effect of silane-functionalized graphene nanoplatelets on the mechanical properties and thermal conductivity of reinforced silicone rubber was studied, with experimental results matching theoretical predictions.

JOURNAL OF MATERIALS SCIENCE (2022)

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Article Chemistry, Physical

Localized Spectroelectrochemical Identification of Basal Plane and Defect-Related Charge-Transfer Processes in Graphene

Martin Jindra et al.

Summary: This study introduces a localized spectroelectrochemical method that addresses the issue of distinguishing processes at the edges/defects from those at the intact basal plane. By comparing the electrochemical and spectral responses of monolayer graphene samples with different levels of disorder, it is discovered that both intact and defective areas contribute to the Raman G band shifts and cyclic voltammetry using the hexaammineruthenium complex. Consequently, two independent electron transfer processes coexist in one sample, but are restricted to defect-free and defect-rich areas, respectively.

JOURNAL OF PHYSICAL CHEMISTRY LETTERS (2022)

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Article Nanoscience & Nanotechnology

Spatially mapping thermal transport in graphene by an optothermal method

Oliver Braun et al.

Summary: Mapping the thermal transport properties at the nanoscale is crucial for optimizing heat conduction in nanoscale devices. Existing methods for determining thermal conductivity provide average values, neglecting local variations. In this study, we propose a method that combines confocal Raman thermometry with finite-element calculations to spatially assess the thermal conductivity of suspended graphene. We demonstrate the effectiveness of our method by obtaining two-dimensional thermal conductivity maps of pristine and irradiated graphene. This approach opens up possibilities for studying the thermal conductivity of other layered materials, which is important for designing nanoscale thermal circuits.

NPJ 2D MATERIALS AND APPLICATIONS (2022)

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Article Nanoscience & Nanotechnology

Machine Learning Determination of the Twist Angle of Bilayer Graphene by Raman Spectroscopy: Implications for van der Waals Heterostructures

Pablo Solis-Fernandez et al.

Summary: In this work, the use of machine learning techniques for the automated classification of the Raman spectrum of twisted bilayer graphene (tBLG) into a selected range of twist angles is proposed. The ML classification is low computationally demanding and provides fast and accurate results with a high agreement with the manual labeling of the spectra.

ACS APPLIED NANO MATERIALS (2022)

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Article Materials Science, Composites

Interfacial energy dissipation in bio-inspired graphene nanocomposites

Sijia Hao et al.

Summary: Bio-inspired nanocomposites were fabricated using GO-based fillers and their interfacial energy dissipation during cyclic deformation was studied. It was found that the presence of functional groups reduced the interfacial energy dissipation in the elastic regime, but increased it with strain. This study provides new insights for the fabrication and evaluation of bio-inspired nanocomposites.

COMPOSITES SCIENCE AND TECHNOLOGY (2022)

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Article Chemistry, Physical

Preferential self-healing at grain boundaries in plasma-treated graphene

P. Vinchon et al.

Summary: Hyperspectral Raman imaging is used to visualize defects in polycrystalline graphene under ion bombardment, showing zero-dimensional and one-dimensional defects in grains and at grain boundaries, respectively, and preferential self-healing at the grain boundaries.

NATURE MATERIALS (2021)

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Article Nanoscience & Nanotechnology

Efficient Mechanical Stress Transfer in Multilayer Graphene with a Ladder-like Architecture

Aristotelis P. Sgouros et al.

Summary: The study demonstrates that embedding few graphene flakes into polymer matrices in a ladder-like morphology allows for significant deformation. This unique architecture prevents interlayer sliding and optimizes strain transfer efficiency, indicating potential for various applications.

ACS APPLIED MATERIALS & INTERFACES (2021)

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Article Chemistry, Multidisciplinary

Intense Raman D Band without Disorder in Flattened Carbon Nanotubes

Emmanuel Picheau et al.

Summary: Above a critical diameter, carbon nanotubes collapse into flattened forms, leading to unique Raman spectra changes. The presence of edge cavities and curvature changes near the edges activate a D band despite overall continuity in the structure. The differing perspectives of chemists and physicists on defects in carbon structures may lead to confusion for researchers in nanotechnologies.

ACS NANO (2021)

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Article Chemistry, Physical

Raman study of D* band in graphene oxide and its correlation with reduction

A. Young Lee et al.

Summary: The study investigates the relationship between the intensity ratio of D* to G band and the reduction of graphene oxide (GO) to evaluate the degree of reduction of rGO. Spectral analysis and systematic research revealed a strong linkage between the D*/G intensity ratio and the C/O atomic ratio, which provides an indicator of the quality of rGO for optimal performance in applications.

APPLIED SURFACE SCIENCE (2021)

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Article Materials Science, Composites

A novel π bridging method to graft graphene oxide onto carbon fiber for interfacial enhancement of epoxy composites

Fei Yan et al.

Summary: A novel method of pi bridging between graphene oxide and carbon fiber was presented without the need for chemical treatment, resulting in improved performance of composites without damaging the carbon fiber. The introduced bridging agent significantly increased interlaminar shear strength, transverse fiber bundle strength, and interfacial shear strength of the composites.

COMPOSITES SCIENCE AND TECHNOLOGY (2021)

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Article Chemistry, Physical

Inherent strains in chemical-vapor-deposited bilayer graphene on Cu

Jinglan Liu et al.

Summary: The electrical properties of bilayer graphene are strongly influenced by external forces. Raman spectroscopy and molecular dynamics simulations were used to study the strain states of bilayer graphene synthesized by chemical vapor deposition, revealing that twisted BLG is under compression with the bottom layer experiencing larger compressive strain, while AB-stacked BLG has its top layer compressed and bottom layer tensile.

CARBON (2021)

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Article Chemistry, Physical

Temperature dependent Raman modes of reduced graphene oxide: Effect of anharmonicity, crystallite size and defects

Meenu Sharma et al.

Summary: The temperature dependent Raman spectroscopy of reduced graphene oxide (rGO) reveals the combined effect of anharmonicity, crystallite size, and defects on the peak positions and line widths of G- and D- modes. The dominance of true-anharmonic part in shifting the peak positions is indicated by theoretical models. The contributions of electron-phonon coupling, anharmonicity, and defects to the temperature dependent variation of line width are discussed.

CARBON (2021)

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Article Physics, Applied

Raman spectroscopy for carbon nanotube applications

A. Jorio et al.

Summary: This tutorial review presents the use of Raman spectroscopy in carbon nanotube applications, discussing how to utilize Raman spectral features for controlling and characterizing nanotube properties, and introducing advanced techniques to enhance the relevance of Raman spectroscopy in this field.

JOURNAL OF APPLIED PHYSICS (2021)

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Article Chemistry, Multidisciplinary

Fundamental Insights into Graphene Strain Sensing

Mufeng Liu et al.

Summary: The study demonstrates that mono-/few-layer graphene are good candidates for strain sensing with high spatial resolution to evaluate features <100 nm. The sensors can monitor the initiation and evolution of crazes, and enable evaluation of high local strain in graphene.

NANO LETTERS (2021)

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Article Mechanics

A novel physicomechanical approach to dispersion of carbon nanotubes in polypropylene composites

G. M. Kim et al.

Summary: A novel physicomechanical technique was proposed to disperse carbon nanotube particles for fabricating electrically conducive polymer composites, utilizing a combination of silica fume and ultrasonication to generate physical shock to carbon nanotube agglomerates and significantly improve dispersion. This technique demonstrated significantly lower electrical resistivity in polypropylene composites compared to previous studies using carbon nanotubes.

COMPOSITE STRUCTURES (2021)

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Article Materials Science, Composites

Remarkably improved interfacial adhesion of pitch-based carbon fiber composites by constructing a synergistic hybrid network at interphase

Qing Wu et al.

Summary: The study introduces a novel strategy of incorporating a ternary organic material on fiber surface to increase the interfacial shear strength of pitch-based carbon fiber composites. By forming a solid connection and enhancing surface energy, a synergistic hybrid network is created, leading to a significant increase in interfacial shear strength. The findings provide unique insights for addressing the weak interface in pitch-based carbon fiber composites.

COMPOSITES SCIENCE AND TECHNOLOGY (2021)

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Article Materials Science, Multidisciplinary

Seamless control of the electrical property of carbon nanotube buckypapers by a simple mixing approach

Taiyo Shimizu et al.

Summary: The study focuses on controlling the electrical conductivities of CNT buckypapers by utilizing mixed dispersions of different types of CNTs, achieving seamless transitions between two sole counterparts. Additionally, an intriguing correlation between electrical conductivities and thermal diffusivities of the obtained buckypapers was discovered. This finding could provide valuable insights for applications involving both electrical and thermal conduction by CNTs.

MATERIALS LETTERS (2021)

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Article Thermodynamics

Blue hydrogen and carbon nanotube production via direct catalytic decomposition of methane in fluidized bed reactor: Capture and extraction of carbon in the form of CNTs

Kaushal R. Parmar et al.

Summary: This study presents a regenerative approach for producing blue hydrogen and carbon nanotubes from natural gas, utilizing a synthesized catalyst in a fluidized bed reactor. The catalyst design considered fluidized bed reactor hydrodynamics and CNT extraction, with the catalyst successfully regenerated using ultrasonication. Advanced characterization tools such as 3D-Raman mapping were used to analyze and confirm the quality of the CNTs produced.

ENERGY CONVERSION AND MANAGEMENT (2021)

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Article Multidisciplinary Sciences

Localization of lattice dynamics in low-angle twisted bilayer graphene

Andreij C. Gadelha et al.

Summary: The twisted bilayer graphene undergoes self-organized lattice reconstruction, resulting in the formation of a superlattice that modulates vibrational and electronic structures, leading to phenomena such as strong correlations and superconductivity. Although experimental techniques and theoretical models face challenges in observing and describing these effects, nano-Raman spectroscopy can localize some vibrational modes and provide insights into the effects of electron-phonon coupling on the material properties.

NATURE (2021)

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Article Multidisciplinary Sciences

Tunable strongly coupled superconductivity in magic-angle twisted trilayer graphene

Jeong Min Park et al.

Summary: Moire superlattices have become a platform for studying correlated physics and superconductivity with unprecedented tunability. This study on magic-angle twisted trilayer graphene reveals a better tunability of electronic structure and superconducting properties than magic-angle twisted bilayer graphene, with implications for the understanding of strongly coupled superconductivity. The results suggest that the system can be electrically tuned close to the crossover to a two-dimensional Bose-Einstein condensate, indicating the potential for revolutionizing applications of superconductivity.

NATURE (2021)

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Article Chemistry, Multidisciplinary

Study of Thermal Expansion Coefficient of Graphene via Raman Micro-Spectroscopy: Revisited

Qianchi Feng et al.

Summary: The study reveals the significant impact of out-of-plane coupling on thermal properties of graphene, as well as the reduction of density of states for longer wavelength out-of-plane vibrations when graphene is supported on an alkane substrate. The negative thermal expansion coefficient of freestanding graphene decreases when out-of-plane rippling is suppressed.

SMALL (2021)

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Article Multidisciplinary Sciences

Controlling the thermal conductivity of multilayer graphene by strain

Kaito Nakagawa et al.

Summary: This study investigates the effects of biaxial tensile strain on the thermal conductivity of graphene, finding that the thermal conductivity decreases with strain. This discovery opens up possibilities for using graphene as high-efficiency thermal switches and diodes in future thermal management devices.

SCIENTIFIC REPORTS (2021)

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Article Nanoscience & Nanotechnology

Abnormal Raman Characteristics of Graphene Originating from Contact Interface Inhomogeneity

Chaochen Xu et al.

Summary: The study investigates the Raman characteristics of graphene derived from CVD when transferred onto polymer substrates using in situ Raman spectroscopy and a tensile test system. It reveals that the Raman 2D-peak position of CVD graphene can shift nonlinearly with applied strain, resulting in a significantly lower RSS coefficient than the theoretical prediction. The abnormal behavior is attributed to nanometer-scale inhomogeneity of the graphene/substrate contact interface, which is essential for correct interpretation of data obtained by Raman or other spectroscopies based on homogenized laser signals.

ACS APPLIED MATERIALS & INTERFACES (2021)

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Article Engineering, Multidisciplinary

π - π interaction between carbon fibre and epoxy resin for interface improvement in composites

Lei Zeng et al.

Summary: This study introduces a new biomimetic method for modifying carbon fiber surfaces to enhance bonding with epoxy resin systems. By forming a nano-thin surface-adherent polydopamine layer and grafting graphene oxide, the interfacial strength of the composites was increased significantly. The research demonstrated the potential of pi-pi interaction-based fiber modification in improving the crack resistance of fiber reinforced polymer composites.

COMPOSITES PART B-ENGINEERING (2021)

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Article Engineering, Multidisciplinary

Exploiting the synergic strengthening effects of stacking faults in carbon nanotubes reinforced aluminum matrix composites for enhanced mechanical properties

Baisong Guo et al.

Summary: CNTs reinforced Al matrix composites containing high-density stacking faults were successfully fabricated, with the highest tensile strength and good ductility achieved at 1 vol% CNTs content. The strengthening mechanisms mainly include Orowan looping and stacking fault strengthening, which depend on the CNTs content. The reported microstructure design and control are informative for improving the mechanical properties of CNTs reinforced metal matrix composites.

COMPOSITES PART B-ENGINEERING (2021)

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Article Materials Science, Composites

Comparative study of multiwall carbon nanotube nanocomposites by Raman, SEM, and XPS measurement techniques

Yanmei Piao et al.

Summary: This study evaluated the effectiveness of XPS, Raman spectroscopy, and SEM methods on MWCNT-epoxy nanocomposite samples, finding a positive correlation between signal intensity and MWCNT mass loading. The results showed that these methods were capable of detecting MWCNTs at different concentrations and demonstrated good comparability among them.

COMPOSITES SCIENCE AND TECHNOLOGY (2021)

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Review Chemistry, Multidisciplinary

Review on Techniques for Thermal Characterization of Graphene and Related 2D Materials

Jing Liu et al.

Summary: Research on thermal transport in 2D materials, particularly focusing on high thermal conductivity in graphene, has been boosted. However, large discrepancies in thermal properties obtained from experiments require careful examination due to various factors. Further improvements in thermal characterization techniques are necessary for investigating energy transport in 2D materials.

NANOMATERIALS (2021)

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Article Polymer Science

Relationship between crystalline structure of polyamide 6 within carbon fibers and their mechanical properties studied using Micro-Raman spectroscopy

Hideyuki Uematsu et al.

Summary: The research found that the surface profile of carbon fibers has a significant impact on the impact strength and debonding appearance of polyamide 6 composites. Micro-Raman spectroscopy analysis revealed that the polymorphism of the PA6 matrix varied between the interface and bulk region, depending on the surface profiles of the carbon fibers.

POLYMER (2021)

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Review Chemistry, Multidisciplinary

Shear and Breathing Modes of Layered Materials

Giovanni Pizzi et al.

Summary: This study focuses on the Raman and infrared spectroscopy of layered materials, presenting a general approach to predict spectroscopic fan diagrams for multilayers composed of identical layers. The method combines a description of normal modes with symmetry arguments to identify optically active modes and provide diagrams for any stack of identical layers.

ACS NANO (2021)

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Article Chemistry, Multidisciplinary

Real-Time Multiscale Monitoring and Tailoring of Graphene Growth on Liquid Copper

Maciej Jankowski et al.

Summary: Real-time monitoring of graphene growth on liquid copper has allowed for accurate control of growth parameters and the transition from continuous polycrystalline film to defect-free single crystals. These results have broad implications for studying and tailoring 2D material formation processes on LMCats under CVD growth conditions.

ACS NANO (2021)

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Article Chemistry, Physical

Environment friendly dual-frequency ultrasonic exfoliation of few-layer graphene

Anastasia Tyurnina et al.

Summary: The ultrasound-aided liquid phase exfoliation of graphene in pure water is environmentally friendly and can achieve a high graphene yield. By using a combination of high and low frequency ultrasound sources, larger and more uniform graphene flakes can be produced. Controlling acoustic pressure and utilizing a dual frequency ultrasonic source are critical in optimizing the quality and yield of the graphene exfoliation process.

CARBON (2021)

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Article Engineering, Manufacturing

High-strength carbon nanotube/epoxy resin composite film from a controllable cross-linking reaction

Jun Cong Long et al.

Summary: A facile and effective method was proposed for preparing high-strength CNT/EP composite films, achieving a tensile strength of 2.5 GPa, which is about 5 times that of the raw CNT film. This approach may offer an effective strategy for the preparation of high-performance CNT composite materials.

COMPOSITES PART A-APPLIED SCIENCE AND MANUFACTURING (2021)

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Article Materials Science, Composites

An improved analytical model for inversely determining multiple interfacial parameters from single fiber micro-Raman and fragmentation tests

Man Zhu et al.

Summary: The study develops an analytical model for accurately predicting stress transfer near a fiber break and simultaneously determining three key interfacial parameters. Through validation with finite element simulations, the model demonstrates good ability in inversely identifying interfacial properties.

COMPOSITES SCIENCE AND TECHNOLOGY (2021)

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Article Materials Science, Multidisciplinary

Quantitative analysis of Raman spectral parameters for carbon fibers: practical considerations and connection to mechanical properties

Z. E. Brubaker et al.

Summary: The literature lacks a consistent, robust predictive relationship between mechanical properties of carbon fibers and spectral parameters due to the use of numerous fitting functions. This study presents a comprehensive approach combining experimental data, numerical analysis, and statistical evaluation to address this gap, offering insights into the correlations between mechanical properties and Raman spectral parameters in carbon fibers.

JOURNAL OF MATERIALS SCIENCE (2021)

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Article Chemistry, Physical

Polarized Raman Spectroscopy for Determining Crystallographic Orientation of Low-Dimensional Materials

Bo Xu et al.

Summary: This article introduces Raman spectroscopy as a fast and nondestructive characterization technique, discusses the application of polarized Raman spectroscopy in determining the crystallographic orientation of materials, and explains the experimental principles and methods using linearly polarized and circularly polarized Raman scattering techniques.

JOURNAL OF PHYSICAL CHEMISTRY LETTERS (2021)

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Article Chemistry, Multidisciplinary

Mechanical Robustness of Metal Nanocomposites Rendered by Graphene Functionalization

Lei Zhao et al.

Summary: Nanocarbon materials like graphene and carbon nanotubes are considered effective in reinforcing metals, and the nature of interfaces plays a significant role in the mechanical behavior of nanocarbon-metal composites. By studying nanolaminated graphene-aluminum composites, it was found that composites with an intermediate level of graphene functionalization exhibited the best strength-ductility synergy.

NANO LETTERS (2021)

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Article Nanoscience & Nanotechnology

Wide-Field Super-Resolved Raman Imaging of Carbon Materials

Mingqun Wang et al.

Summary: SIRM is a high-throughput super-resolution Raman imaging method with spatial resolution up to 80 nm and spectral resolution up to 50 cm(-1). This technique enables fast large-scale characterization of nanomaterials, with imaging time of specific Raman bands reduced to seconds.

ACS PHOTONICS (2021)

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Article Materials Science, Multidisciplinary

Interlayer and interfacial stress transfer in hBN nanosheets

Weimiao Wang et al.

Summary: Research has shown that hexagonal boron nitride nanosheets (BNNSs) exhibit higher internal interlayer stress transfer efficiency and better interfacial stress transfer performance compared to graphene, resulting in better mechanical reinforcement in polymer-based nanocomposites.

2D MATERIALS (2021)

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Article Engineering, Electrical & Electronic

Sub-10-nm graphene nanoribbons with atomically smooth edges from squashed carbon nanotubes

Changxin Chen et al.

Summary: Sub-10-nm-wide semiconducting graphene nanoribbons with atomically smooth closed edges can be produced by squashing carbon nanotubes using a high-pressure and thermal treatment. The resulting nanoribbons exhibit high mobilities and can be used to fabricate field-effect transistors with high performance.

NATURE ELECTRONICS (2021)

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Article Chemistry, Multidisciplinary

Effect of graphene flake size on functionalisation: quantifying reaction extent and imaging locus with single Pt atom tags

Noelia Rubio et al.

Summary: The study shows that the locus of functionalisation on graphene-related materials and the progress of the reaction strongly depend on the starting feedstock. Experiments with five characteristically different graphite sources reveal an increase in grafting ratio and an improvement in grafting stoichiometry as flake radius decreases. Raman spectrum imaging indicates that grafting is directed towards flake edges.

CHEMICAL SCIENCE (2021)

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Article Chemistry, Physical

Studying 2D materials with advanced Raman spectroscopy: CARS, SRS and TERS

Leandro M. Malard et al.

Summary: This article reviews the use of advanced Raman spectroscopy techniques to study various 2D materials, discussing results on graphene, hexagonal boron-nitride, and transition metal di- and mono-chalcogenides. The study provides perspectives for future research in this early-stage field, including similar studies on unexplored 2D systems and open questions.

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2021)

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Article Polymer Science

Analysis of carbon fiber structure based on dynamic laser Raman spectroscopy

Zhulin Sun et al.

Summary: The thermal conductivity and Young's modulus of carbon fibers are intrinsic properties that determine their properties, with different types of carbon fibers exhibiting different characteristics, such as the higher thermal conductivity of mesophase pitch-based carbon fiber compared to polyacrylonitrile and rayon-based carbon fibers.

JOURNAL OF APPLIED POLYMER SCIENCE (2021)

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Article Chemistry, Physical

Raman spectroscopy on hydrogenated graphene under high pressure

Teerachote Pakornchote et al.

CARBON (2020)

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Article Chemistry, Physical

Effect of high temperature treatment on the microstructure and elastoplastic properties of polyacrylonitrile-based carbon fibers

Fenghao Yang et al.

CARBON (2020)

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Article Chemistry, Physical

Experimental measurements on the thermal conductivity of strained monolayer graphene

Ming Guo et al.

CARBON (2020)

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Article Chemistry, Physical

PMMA-grafted graphene nanoplatelets to reinforce the mechanical and thermal properties of PMMA composites

Cristina Valles et al.

CARBON (2020)

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Article Chemistry, Physical

Understanding cooperative loading in carbon nanotube fibres through in-situ structural studies during stretching

Juan C. Fernandez-Toribio et al.

CARBON (2020)

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Review Chemistry, Multidisciplinary

Chirality Pure Carbon Nanotubes: Growth, Sorting, and Characterization

Feng Yang et al.

CHEMICAL REVIEWS (2020)

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Article Engineering, Manufacturing

A filler-matrix interaction model for the large deformation response of graphene nanocomposite - A PVA-GO nanocomposite example

Ebrahim Sadeghpour et al.

COMPOSITES PART A-APPLIED SCIENCE AND MANUFACTURING (2020)

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Article Polymer Science

Graphene-based polymer composites with ultra-high in-plane thermal conductivity: A comparison study between optothermal Raman spectroscopy and laser flash method

Ali Tarhini et al.

JOURNAL OF APPLIED POLYMER SCIENCE (2020)

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Article Chemistry, Multidisciplinary

Few-Wall Carbon Nanotube Coils

Dekel Nakar et al.

NANO LETTERS (2020)

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Article Nanoscience & Nanotechnology

Large-area single-crystal AB-bilayer and ABA-trilayer graphene grown on a Cu/Ni(111) foil

Ming Huang et al.

NATURE NANOTECHNOLOGY (2020)

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Article Materials Science, Composites

Micromechanics analysis of carbon fiber/epoxy microdroplet composite under UV light irradiation by micro-Raman spectroscopy

Xiu Fu et al.

POLYMER COMPOSITES (2020)

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Article Multidisciplinary Sciences

Liquids relax and unify strain in graphene

Liubov A. Belyaeva et al.

NATURE COMMUNICATIONS (2020)

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Article Physics, Applied

Raman spectroscopy study of sp2 to sp3 transition in bilayer graphene under high pressures

Zhuchen Tao et al.

APPLIED PHYSICS LETTERS (2020)

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Article Chemistry, Physical

Raman spectroscopy analysis of number of layers in mass-produced graphene flakes

Diego L. Silva et al.

CARBON (2020)

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Article Chemistry, Physical

Assessing the structural properties of graphitic and non-graphitic carbons by Raman spectroscopy

Dominique B. Schuepfer et al.

CARBON (2020)

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Article Multidisciplinary Sciences

Aligned, high-density semiconducting carbon nanotube arrays for high-performance electronics

Lijun Liu et al.

SCIENCE (2020)

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Article Multidisciplinary Sciences

Tunable macroscale structural superlubricity in two-layer graphene via strain engineering

Charalampos Androulidakis et al.

NATURE COMMUNICATIONS (2020)

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Article Chemistry, Multidisciplinary

Raman Fingerprints of Graphene Produced by Anodic Electrochemical Exfoliation

Vaiva Nagyte et al.

NANO LETTERS (2020)

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Article Chemistry, Physical

Raman Metrics for Molybdenum Disulfide and Graphene Enable Statistical Mapping of Nanosheet Populations

Aline Amorim Graf et al.

CHEMISTRY OF MATERIALS (2020)

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Article Chemistry, Physical

Machine-learning models for Raman spectra analysis of twisted bilayer graphene

Natalya Sheremetyeva et al.

CARBON (2020)

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Review Thermodynamics

Raman-based Nanoscale Thermal Transport Characterization: A Critical Review

Shen Xu et al.

INTERNATIONAL JOURNAL OF HEAT AND MASS TRANSFER (2020)

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Article Materials Science, Multidisciplinary

Strain engineering in monolayer WS2and WS2nanocomposites

Fang Wang et al.

2D MATERIALS (2020)

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Article Physics, Applied

Quantifying the interfacial load transfer in electrospun carbon nanotube polymer nanocomposite microfibers by using in situ Raman micromechanical characterization techniques

Ohood Q. Alsmairat et al.

JOURNAL OF PHYSICS D-APPLIED PHYSICS (2020)

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Article Chemistry, Physical

Adverse effect of mesophase pitch draw-down ratio on carbon fiber strength

Victor Bermudez et al.

CARBON (2020)

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Article Chemistry, Physical

Ultrasonic exfoliation of graphene in water: A key parameter study

Anastasia Tyurnina et al.

CARBON (2020)

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Article Multidisciplinary Sciences

Electronic phase separation in multilayer rhombohedral graphite

Yanmeng Shi et al.

NATURE (2020)

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Article Multidisciplinary Sciences

Super-durable ultralong carbon nanotubes

Yunxiang Bai et al.

SCIENCE (2020)

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Article Physics, Applied

Linkage Between Micro- and Nano-Raman Spectroscopy of Defects in Graphene

Cassiano Rabelo et al.

PHYSICAL REVIEW APPLIED (2020)

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Article Materials Science, Composites

Mapping the residual strain of carbon nanotubes in DWCNT/epoxy nanocomposites after tensile load using Raman microscopy

Susanna Laurenzi et al.

COMPOSITES COMMUNICATIONS (2020)

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Review Optics

Strain engineering of 2D semiconductors and graphene: from strain fields to band-structure tuning and photonic applications

Zhiwei Peng et al.

LIGHT-SCIENCE & APPLICATIONS (2020)

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Article Engineering, Multidisciplinary

Understanding interlaminar toughening of unidirectional CFRP laminates with carbon nanotube veils

Yunfu Ou et al.

COMPOSITES PART B-ENGINEERING (2020)

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Article Nanoscience & Nanotechnology

Engineering the Interphase of Single Wall Carbon Nanotubes/Polyacrylonitrile Nanocomposite Fibers with Poly(methyl methacrylate) and Its Effect on Filler Dispersion, Filler-Matrix Interactions, and Tensile Properties

Pedro J. Arias-Monje et al.

ACS APPLIED NANO MATERIALS (2020)

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Article Chemistry, Physical

The taxonomy of graphite nanoplatelets and the influence of nanocomposite processing

Zheling Li et al.

CARBON (2019)

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Article Chemistry, Physical

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Stress transfer in polyacrylonitrile/carbon nanotube composite fibers

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Failure Processes in Embedded Monolayer Graphene under Axial Compression

Charalampos Androulidakis et al.

SCIENTIFIC REPORTS (2014)

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Excitation Energy Dependent Raman Signatures of ABA- and ABC-stacked Few-layer Graphene

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SCIENTIFIC REPORTS (2014)

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Interfacial Stress Transfer in Graphene Oxide Nanocomposites

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ACS APPLIED MATERIALS & INTERFACES (2013)

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Scanning-Raman-Microscopy for the Statistical Analysis of Covalently Functionalized Graphene

Jan M. Engiert et al.

ACS NANO (2013)

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Reversible Loss of Bernal Stacking during the Deformation of Few-Layer Graphene in Nanocompo sites

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ACS NANO (2013)

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Near-infrared fluorescent single walled carbon nanotube-chitosan composite: Interfacial strain transfer efficiency assessment

Mini Mol Menamparambath et al.

APPLIED PHYSICS LETTERS (2013)

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The effect of nanostructure upon the deformation micromechanics of carbon fibres

Fumihiko Tanaka et al.

CARBON (2013)

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Raman spectroscopic imaging of graphene dispersion in polymer composites

S. Ali Shojaee et al.

CARBON (2013)

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The use of a carbon nanotube sensor for measuring strain by micro-Raman spectroscopy

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CARBON (2013)

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CARBON (2013)

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Single carbon fiber fracture embedded in an epoxy matrix modified by nanoparticles

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COMPOSITES SCIENCE AND TECHNOLOGY (2013)

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Graphene oxide and base-washed graphene oxide as reinforcements in PMMA nanocomposites

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COMPOSITES SCIENCE AND TECHNOLOGY (2013)

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The effect of nanostructure upon the compressive strength of carbon fibres

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JOURNAL OF MATERIALS SCIENCE (2013)

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Rapid Identification of Stacking Orientation in Isotopically Labeled Chemical-Vapor Grown Bilayer Graphene by Raman Spectroscopy

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NANO LETTERS (2013)

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How Graphene Slides: Measurement and Theory of Strain-Dependent Frictional Forces between Graphene and SiO2

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NANO LETTERS (2013)

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Chemical mapping of a single molecule by plasmon-enhanced Raman scattering

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Review Nanoscience & Nanotechnology

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NATURE NANOTECHNOLOGY (2013)

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Raman study on defective graphene: Effect of the excitation energy, type, and amount of defects

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PHYSICAL REVIEW B (2013)

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Graphene-induced crystallinity of bisphenol A polycarbonate in the presence of supercritical carbon dioxide

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A coupled quantum/continuum mechanics study of graphene fracture

Mei Xu et al.

INTERNATIONAL JOURNAL OF FRACTURE (2012)

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Self-alignment and high electrical conductivity of ultralarge graphene oxide-polyurethane nanocomposites

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A Raman Spectroscopy Study on Single-Wall Carbon Nanotube/Polystyrene Nanocomposites: Mechanical Compression Transferred from the Polymer to Single-Wall Carbon Nanotubes

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Phonon and Structural Changes in Deformed Bernal Stacked Bilayer Graphene

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NANO LETTERS (2012)

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NANO LETTERS (2012)

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NANO LETTERS (2012)

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NANO RESEARCH (2012)

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Thermal conductivity of isotopically modified graphene

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NATURE MATERIALS (2012)

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The shear mode of multilayer graphene

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NATURE MATERIALS (2012)

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Raman Spectroscopy Study of Rotated Double-Layer Graphene: Misorientation-Angle Dependence of Electronic Structure

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PHYSICAL REVIEW LETTERS (2012)

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Optical separation of mechanical strain from charge doping in graphene

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NATURE COMMUNICATIONS (2012)

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Raman Characterization of ABA- and ABC-Stacked Trilayer Graphene

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ADVANCED FUNCTIONAL MATERIALS (2011)

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Raman spectroscopy of graphene and carbon nanotubes

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ADVANCES IN PHYSICS (2011)

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ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2011)

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Raman study of interfacial load transfer in graphene nanocomposites

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APPLIED PHYSICS LETTERS (2011)

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Structural heterogeneity and stress distribution in carbon fiber monofilament as revealed by synchrotron micro-beam X-ray scattering and micro-Raman spectral measurements

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CARBON (2011)

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Electrical conductivity and Raman imaging of double wall carbon nanotubes in a polymer matrix

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COMPOSITES SCIENCE AND TECHNOLOGY (2011)

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Simultaneous global and local strain sensing in SWCNT-epoxy composites by Raman and impedance spectroscopy

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COMPOSITES SCIENCE AND TECHNOLOGY (2011)

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Pressure-Induced Collapse in Double-Walled Carbon Nanotubes: Chemical and Mechanical Screening Effects

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JOURNAL OF PHYSICAL CHEMISTRY C (2011)

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Temperature effects on the Raman spectra of graphenes: dependence on the number of layers and doping

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JOURNAL OF PHYSICS-CONDENSED MATTER (2011)

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Intercalation of Few-Layer Graphite Flakes with FeCl3: Raman Determination of Fermi Level, Layer by Layer Decoupling, and Stability

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JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2011)

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Raman Signature of Graphene Superlattices

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NANO LETTERS (2011)

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NANO LETTERS (2011)

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NANOSCALE (2011)

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Control and characterization of individual grains and grain boundaries in graphene grown by chemical vapour deposition

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NATURE MATERIALS (2011)

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Strain-Dependent Splitting of the Double-Resonance Raman Scattering Band in Graphene

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PHYSICAL REVIEW LETTERS (2011)

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NATURE COMMUNICATIONS (2011)

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ADVANCED MATERIALS (2010)

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CARBON (2010)

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CARBON (2010)

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JOURNAL OF MATERIALS SCIENCE (2010)

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JOURNAL OF MATERIALS SCIENCE (2010)

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JOURNAL OF RAMAN SPECTROSCOPY (2010)

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NANO LETTERS (2010)

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NANO LETTERS (2010)

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NANO LETTERS (2010)

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Thermal Transport in Suspended and Supported Monolayer Graphene Grown by Chemical Vapor Deposition

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NANO LETTERS (2010)

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NANO LETTERS (2010)

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PHYSICA STATUS SOLIDI B-BASIC SOLID STATE PHYSICS (2010)

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Evolution of the Raman spectra from single-, few-, and many-layer graphene with increasing disorder

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PHYSICAL REVIEW B (2010)

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Article Polymer Science

Characterization of the adhesion of single-walled carbon nanotubes in poly (p-phenylene terephthalamide) composite fibres

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Two-Dimensional Phonon Transport in Supported Graphene

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SCIENCE (2010)

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SMALL (2010)

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ACS NANO (2009)

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Effect of fatigue on the interface integrity of unidirectional Cf-reinforced epoxy resin composites

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ACTA MATERIALIA (2009)

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ADVANCED MATERIALS (2009)

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ADVANCED MATERIALS (2009)

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Raman spectroscopic evidence for interfacial interactions in poly(bithiophene)/single-walled carbon nanotube composites

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CARBON (2009)

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Chemical analysis of graphene oxide films after heat and chemical treatments by X-ray photoelectron and Micro-Raman spectroscopy

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CARBON (2009)

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SWNT composite coatings as a strain sensor on glass fibres in model epoxy composites

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COMPOSITES SCIENCE AND TECHNOLOGY (2009)

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JOURNAL OF PHYSICAL CHEMISTRY C (2009)

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High-Strength Composite Fibers: Realizing True Potential of Carbon Nanotubes in Polymer Matrix through Continuous Reticulate Architecture and Molecular Level Couplings

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NANO LETTERS (2009)

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Raman Spectroscopy of Graphene Edges

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NANO LETTERS (2009)

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High-pressure Raman spectroscopy of graphene

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PHYSICAL REVIEW B (2009)

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Uniaxial strain in graphene by Raman spectroscopy: G peak splitting, Gruneisen parameters, and sample orientation

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PHYSICAL REVIEW B (2009)

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Raman spectroscopy in graphene

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PHYSICS REPORTS-REVIEW SECTION OF PHYSICS LETTERS (2009)

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Phonon softening and crystallographic orientation of strained graphene studied by Raman spectroscopy

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PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA (2009)

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Subjecting a Graphene Monolayer to Tension and Compression

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SMALL (2009)

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ACS NANO (2008)

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Edge chirality determination of graphene by Raman spectroscopy

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APPLIED PHYSICS LETTERS (2008)

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Measuring the degree of stacking order in graphite by Raman spectroscopy

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CARBON (2008)

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Stress transfer of single fiber/microdroplet tensile test studied by micro-Raman spectroscopy

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COMPOSITES PART A-APPLIED SCIENCE AND MANUFACTURING (2008)

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Raman mapping investigation of graphene on transparent flexible substrate: The strain effect

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JOURNAL OF PHYSICAL CHEMISTRY C (2008)

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Chirality-Dependent Raman Frequency Variation of Single-Walled Carbon Nanotubes under Uniaxial Strain

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JOURNAL OF PHYSICAL CHEMISTRY C (2008)

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Strong Polarization Dependence of Double-Resonant Raman Intensities in Graphene

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NANO LETTERS (2008)

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Superior thermal conductivity of single-layer graphene

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NANO LETTERS (2008)

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Raman spectra of misoriented bilayer graphene

P. Poncharal et al.

PHYSICAL REVIEW B (2008)

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Reduction of Fermi velocity in folded graphene observed by resonance Raman spectroscopy

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PHYSICAL REVIEW B (2008)

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Raman spectroscopy of epitaxial graphene on a SiC substrate

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PHYSICAL REVIEW B (2008)

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Measurement of the elastic properties and intrinsic strength of monolayer graphene

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SCIENCE (2008)

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Stress transfer in multi-walled carbon nanotubes

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COMPOSITES SCIENCE AND TECHNOLOGY (2007)

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Ab initio calculation of ideal strength and phonon instability of graphene under tension

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PHYSICAL REVIEW B (2007)

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NANO LETTERS (2007)

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Article Nanoscience & Nanotechnology

Deformation of isolated single-wall carbon nanotubes in electrospun polymer nanofibres

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NANOTECHNOLOGY (2007)

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Synthesis of graphene-based nanosheets via chemical reduction of exfoliated graphite oxide

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CARBON (2007)

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Monitoring oxidation of multiwalled carbon nanotubes by Raman spectroscopy

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JOURNAL OF RAMAN SPECTROSCOPY (2007)

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Effect of residual stresses upon the Raman radial breathing modes of nanotubes in epoxy composites

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COMPOSITES SCIENCE AND TECHNOLOGY (2007)

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Raman scattering of carbon nanotube bundles under axial strain and strain-induced debundling

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PHYSICAL REVIEW B (2007)

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Raman spectral probing of electronic transition energy Eii variation of individual SWNTs under torsional strain

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NANO LETTERS (2007)

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The rise of graphene

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NATURE MATERIALS (2007)

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Raman spectra variation of partially suspended individual single-walled carbon nanotubes

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JOURNAL OF PHYSICAL CHEMISTRY C (2007)

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Effect of nanotube functionalization on the coefficient of thermal expansion of nanocomposites

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ADVANCED FUNCTIONAL MATERIALS (2007)

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Temperature dependence of the Raman spectra of graphene and graphene multilayers

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NANO LETTERS (2007)

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Processing and characterization of extruded drawn MWNT-PAN composite filaments

Linda Vaisman et al.

COMPOSITES PART A-APPLIED SCIENCE AND MANUFACTURING (2007)

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Raman scattering from high-frequency phonons in supported n-graphene layer films

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NANO LETTERS (2006)

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Raman spectrum of graphene and graphene layers

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PHYSICAL REVIEW LETTERS (2006)

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Analysis of interfacial micromechanics in microdroplet model composites using synchrotron microfocus X-ray diffraction

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COMPOSITES SCIENCE AND TECHNOLOGY (2006)

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