4.7 Article

Enhanced strength-ductility balance of the (CoCrFeNiMn)95.2Al3.2Ti1.6 high-entropy alloy by co-precipitation of the B2 and sigma phases

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ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2023.145039

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High entropy alloy; Co-precipitation; Mechanical properties; Sigma phase; B2 phase

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This study investigated the effect of the co-precipitation of the B2 and & sigma; phases on the mechanical properties of the (CoCrFeNiMn) 95.2Al3.2Ti1.6 high entropy alloy subjected to two-step annealing. The co-precipitation of & sigma; and B2 particles led to the improvement of mechanical properties, including high strength and moderate ductility. The results suggest that the co-precipitation of & sigma; and B2 particles offers a novel microstructure design to optimize the strength-ductility balance of high-entropy alloys.
The present work investigated the effect of the co-precipitation of the B2 and & sigma; phases on the mechanical properties of the (CoCrFeNiMn)95.2Al3.2Ti1.6 high entropy alloy subjected to two-step annealing. The single-step annealed sample at 900 & DEG;C only showed B2 precipitates. Further annealing at 650 and 750 & DEG;C led to the co precipitation of & sigma; and B2 particles. The sizes and fractions of & sigma; and B2 particles increased with increasing annealing temperature. The sample subjected to the second annealing at 750 & DEG;C, with large sizes and fractions of co-precipitated & sigma; and B2 particles, exhibited high strength with maintaining moderate ductility (YS: 561 MPa, UTS: 1005 MPa, TE: 26%). The superior mechanical properties of the sample subjected to the second annealing at 750 & DEG;C could be owing to the co-precipitation hardening, back stress strengthening, joint activation of dislocation plasticity and deformation twinning. The present work offers a novel microstructure design to optimize the strength-ductility balance of high-entropy alloys via the co-precipitation of & sigma; and B2 particles.

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