☆ 4.5 Review

Ultramicroextraction as a miniaturization of the already miniaturized. A step toward nanoextraction and beyond

JOURNAL OF SEPARATION SCIENCE (2023)

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Integrated lab-on-a-chip devices: Fabrication methodologies, transduction system for sensing purposes

Daphika S. Dkhar et al.

Summary: Lab-on-a-chip (LOC) biosensors have attracted research interest for their potential in personal healthcare and disease diagnostics. This review discusses various fabrication methods and techniques for designing LOC sensing devices, as well as the types of transduction systems that play a crucial role in sensing. The detection of analytes, including small molecules, macromolecules, and cells, is comprehensively reviewed with illustrations and tables.

JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS (2023)

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Article Chemistry, Analytical

New challenges in sample preparation: Miniaturized stir bar sorptive dispersive microextraction as a high-throughput and feasible approach for low-availability sample preparation

Cristian Azorin et al.

Summary: This study introduces a miniaturized stir bar sorptive dispersive microextraction (mSBSDME) method for analyzing low-availability samples. The method significantly reduces the amount of sorbent and sample, allowing for fast, affordable, portable, and high-throughput analysis of low-volume samples.

ANALYTICA CHIMICA ACTA (2023)

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Review Chemistry, Analytical

Latest Improvements and Expanding Applications of Solid-Phase Microextraction

Juan Zheng et al.

ANALYTICAL CHEMISTRY (2023)

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Review Chemistry, Analytical

Disposable pipette extraction: A critical review of concepts, applications, and directions

Eduardo Carasek et al.

Summary: The translation introduces a new sample preparation method – Disposable Pipette Extraction (DPX), which achieves rapid and effective extraction of analytes through dynamic mixing and contributes to reducing waste generation and improving laboratory worker safety by using natural materials to replace commercial ones.

ANALYTICA CHIMICA ACTA (2022)

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Article Biochemical Research Methods

Automatic and renewable micro-solid-phase extraction based on bead injection lab-on-valve system for determination of tranexamic acid in urine by UHPLC coupled with tandem mass spectrometry

Sara R. Fernandes et al.

Summary: An automatic micro-solid-phase extraction method using on-line renewable sorbent beads followed by liquid chromatography-tandem mass spectrometry was established for the determination of tranexamic acid in urine. Through computer programming, enhanced precision on time and flow events was achieved. The method was successfully validated and applied to urine samples collected from pediatric patients undergoing scoliosis surgery.

ANALYTICAL AND BIOANALYTICAL CHEMISTRY (2022)

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Review Chemistry, Analytical

Use of green alternative solvents in dispersive liquid-liquid microextraction: A review

Jose Grau et al.

Summary: Dispersive liquid-liquid microextraction is a widely used technique in analytical chemistry field due to its simplicity and rapidity. The operational mode has evolved over time, with changes mainly related to the nature of solvents used. Low-density solvents, ionic liquids, and other alternatives have been proposed as greener options for this method.

JOURNAL OF SEPARATION SCIENCE (2022)

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Article Biochemical Research Methods

A green microfluidic method based liquid phase microextraction for the determination of parabens in human urine samples

Samira Dowlatshah et al.

Summary: A environmentally friendly microfluidic system based on natural deep eutectic solvents immobilized in agarose membranes was developed for extracting parabens from urine samples. The system showed advantages of nontoxic solvents, miniaturized method and biodegradable materials, and was successfully applied for the determination of parabens in urine samples.

JOURNAL OF CHROMATOGRAPHY A (2022)

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The ten principles of green sample preparation

Angela I. Lopez-Lorente et al.

Summary: The ten principles of GSP aim to establish a roadmap for the development of overall greener analytical methodologies by promoting the use of safe solvents/reagents and renewable materials, reducing waste and energy demand, enabling higher sample throughput, procedure simplification/automation, and improving operator safety.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2022)

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Article Chemistry, Analytical

A high-throughput magnetic-based pipette tip microextraction as an alternative to conventional pipette tip strategies: Determination of testosterone in human saliva as a proof-of-concept

Jose Grau et al.

Summary: A novel high-throughput pipette tip microextraction strategy using a magnetic sorbent has been developed, offering satisfactory results with minimal number of aspirating/dispensing cycles, benefiting the ergonomics for the operator. The strategy has been successfully tested for measuring testosterone levels in saliva of volunteers, achieving low limits of detection and quantification, good repeatability, and high relative recoveries. It shows promise for rapid sample analysis and could be further improved with the use of a multichannel pipette.

ANALYTICA CHIMICA ACTA (2022)

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Article Chemistry, Applied

Green, simple analytical method for biogenic amines determination in fruit juice samples using salting-out assisted liquid-liquid microextraction and gas chromatography-mass spectrometry

Anna Rozanska et al.

Summary: Salting-out assisted liquid-liquid microextraction (SALLME) was combined with derivatization procedure to establish a one-step sample pre-treatment approach for rapid analysis of 14 biogenic amines (BAs) in fruit juices. The developed method exhibited satisfactory analytical performance and was suitable for analysis of different berry juice samples.

FOOD CHEMISTRY (2022)

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Review Biochemical Research Methods

Nanoextraction based on surface nanodroplets for chemical preconcentration and determination

Hongyan Wu et al.

Summary: This article presents a review on nanoextraction based on surface nanodroplets, which can continuously extract and enrich target analytes from a sample solution in a continuous flow system. Nanoextraction is characterized by its simplicity in operation, low consumption of organic solvent, and high enrichment factor. The article also summarizes the formation principle and key features of surface nanodroplets, and discusses the major findings of nanoextraction combined with in-droplet chemistry for sensitive and quantitative detection. Lastly, the future trend of nanoextraction is discussed.

BIOMICROFLUIDICS (2022)

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Review Biophysics

Electrified lab on disc systems: A comprehensive review on electrokinetic applications

Vahid Kordzadeh-Kermani et al.

Summary: This review introduces the on-board power supply and electrokinetic applications of electrified-LOD (eLOD) devices. By utilizing electrokinetic phenomena, different microfluids can be propelled, separated, and manipulated. While extensive research exists on stationary platforms, the applications on rotating platforms are still underdeveloped.

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Microscale solid-liquid extraction: A green alternative for determination of n- alkanes in sediments

Pedro Victor Bomfim Bahia et al.

Summary: A green microscale solid-liquid extraction method was developed for the determination of n- alkanes in marine sediments. The method performance was validated and successfully applied to marine sediment samples.

JOURNAL OF CHROMATOGRAPHY A (2022)

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Article Chemistry, Analytical

Miniaturized, green salting-out liquid-liquid microextraction coupled with GC-MS used to evaluate biogenic amines in wine samples

M. Fabjanowicz et al.

Summary: Monitoring the content of biogenic amines in food products, including wine, is crucial for the health and safety of consumers and for quality control. In this study, a fast, sensitive, and easy-to-perform method using simultaneous derivatization and salting-out liquid-liquid microextraction (SALLME) coupled with GC-MS was developed for the determination of biogenic amines in wine samples. The proposed method showed good sensitivity, recovery, and reproducibility, and the biogenic amine index (BAI) was applied to assess the quality of the wines.

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Article Chemistry, Analytical

Polydopamine inner wall-coated hypodermic needle as microextraction device and electrospray emitter for the direct analysis of illicit drugs in oral fluid by ambient mass spectrometry

Carmina Vejar-Vivar et al.

Summary: This study evaluates polydopamine inner wall-coated hypodermic needles as microextraction devices and electrospray ionization emitters for determining illicit drugs in oral fluid samples.

TALANTA (2022)

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Determination of nerve agent biomarkers in human urine by a natural hydrophobic deep eutectic solvent-parallel artificial liquid membrane extraction technique

Khirreddine Bouchouareb et al.

Summary: A method based on PALME combined with LC-MS/MS analysis using natural hydrophobic deep eutectic solvents was developed and applied for the extraction of AMPAs from urine samples. The method showed good sensitivity, high-throughput, greenness, simplicity, and practicality, making it a powerful technique for biomonitoring of people exposed to nerve agents in public health emergencies.

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Review Chemistry, Analytical

Green miniaturized technologies in analytical and bioanalytical chemistry

Arpana Agrawal et al.

Summary: Green miniaturized technologies are essential for downsizing traditional analytical systems and protecting the environment. This review provides a comprehensive overview of the green aspects of miniaturized systems, including reducing sample/solvent volumes, replacing toxic solvents with green alternatives, and minimizing waste generation.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2021)

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Fundamentals and applications of stir bar sorptive dispersive microextraction: A tutorial review

Victor Vallez-Gomis et al.

Summary: SBSDME is a novel microextraction technique that combines the principles of SBSE and DSPE, dispersing magnetic (nano)material into the sample solution through horizontal stirring, leading to improved extraction efficiency. It offers advantages of shorter extraction times and simplified processing in a single approach.

ANALYTICA CHIMICA ACTA (2021)

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Green and sustainable drug analysis-Combining microsampling and microextraction of drugs of abuse

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Summary: A novel method combining microsampling of whole blood containing drugs of abuse with 96-well liquid solution microextraction and UHPLC-MS/MS analysis was evaluated in this study. The method showed extraction recoveries above 70% and quantification limits between 1 and 5 ng/mL, in line with green chemistry principles.

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Pawel Mateusz Nowak et al.

Summary: The concept of White Analytical Chemistry (WAC) extends from Green Analytical Chemistry (GAC) with 12 WAC principles proposed as an alternative to the known 12 GAC principles. WAC considers key criteria affecting the quality of the method, including analytical and practical aspects, aiming for coherence and synergy of analytical, ecological, and practical attributes.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2021)

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Green micro total analysis systems (GμTAS) for environmental samples

Rustem Kecilia et al.

Summary: Micro total analysis systems (μTAS) offer significant advantages over traditional macroscale systems, including reduced energy consumption, faster and cost-effective analytical processes, and shortened analysis time. Furthermore, automation and high throughput capabilities of μTAS can further enhance efficiency.

TRENDS IN ENVIRONMENTAL ANALYTICAL CHEMISTRY (2021)

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A simple and environmentally-friendly method by pipette-tip matrix solid-phase dispersion microextraction coupled with high-performance liquid chromatography for the simultaneous determination of lignans and terpenes

Chu Chu et al.

Summary: An ultra-miniaturized pipette-tip matrix solid-phase dispersion microextraction method using molecular sieve as adsorbent was developed to determine multiple components in a complex Chinese medicine. Optimization of adsorbent and elution solvent types, as well as extraction conditions, showed good analytical performance and environmental advantages.

SUSTAINABLE CHEMISTRY AND PHARMACY (2021)

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Article Biochemical Research Methods

A selective and efficient microfluidic method-based liquid phase microextraction for the determination of sulfonamides in urine samples

Samira Dowlatshah et al.

Summary: Liquid phase microextraction into a microfluidic device has made significant advances in downscaled and miniaturized extraction of sulfonamides. The proposed method using tributyl phosphate as a supported liquid membrane achieved high extraction efficiencies and low detection limits for sulfadiazine, sulfamerazine, sulfamethazine, and sulfamethoxazole. The developed microfluidic device showed great potential for efficient and rapid determination of sulfonamides in urine samples.

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Article Biochemical Research Methods

Modified magnetic-based solvent-assisted dispersive solid-phase extraction: application to the determination of cortisol and cortisone in human saliva

Jose Grau et al.

Summary: A modification of magnetic-based solvent-assisted dispersive solid-phase extraction method was developed for the determination of cortisol and cortisone in saliva samples. The method showed good analytical features with high sensitivity and accuracy, simplicity in operation, and minimal requirement for supporting equipment.

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Article Chemistry, Analytical

Magnetic paper-based sorptive phase for enhanced mass transference in stir membrane environmental samplers

Francisco Antonio Casado-Carmona et al.

Summary: This article introduces the synthesis and application of a magnetic paper-based sorptive phase, which combines the sorption capacity of polyamide with the magnetic behavior of silica shielded Fe3O4 nanoparticles. The material is capable of extracting parabens and tri-closan from swimming pool water samples, with the convenience of easy transportation and on-site extraction. This innovation has the potential to simplify the analytical process by only transporting the sorptive phases, rather than the actual samples, to the lab for final analysis.

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Article Chemistry, Multidisciplinary

Optimization of a miniaturized solid-phase microextraction method followed by gas chromatography mass spectrometry for the determination of twenty four volatile and semivolatile compounds in honey from Galicia (NW Spain) and foreign countries

Lua Vazquez et al.

Summary: An analytical miniaturized methodology based on solid-phase-microextraction coupled with gas chromatography-mass spectrometry has been developed for the identification of compounds in honey samples. By optimizing experimental parameters, the method was successfully validated for its suitability in analyzing a broad range of honey samples.

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Article Biochemical Research Methods

Surface nanodroplet-based nanoextraction from sub-milliliter volumes of dense suspensions

Jae Bem You et al.

Summary: The article introduces a green, fast one-step method called nanoextraction for extraction and detection of target analytes from dense suspensions, achieving a limit of detection for a fluorescent model analyte obtained from particle suspension samples. Research shows that high particle concentration in suspension samples does not reduce extraction efficiency.

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Emerging Extraction Strategies in Analytical Chemistry

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Polyacrylonitrile/MIL-53(Fe) electrospun nanofiber for pipette-tip micro solid phase extraction of nitrazepam and oxazepam followed by HPLC analysis

Shima Amini et al.

MICROCHIMICA ACTA (2020)

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On-chip ion pair-based dispersive liquid-liquid extraction for quantitative determination of histamine H2 receptor antagonist drugs in human urine

Monireh Karami et al.

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Siyuan Di et al.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2020)

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Nanoliter-Scale Droplet-Droplet Microfluidic Microextraction Coupled with MALDI-TOF Mass Spectrometry for Metabolite Analysis of Cell Droplets

Wen-Hua Sun et al.

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Yadollah Yamini et al.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2019)

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Liquid phase microextraction integrated into a microchip device for the extraction of fluoroquinolones from urine samples

Elia Santigosa et al.

MICROCHEMICAL JOURNAL (2019)

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Dorota Wianowska et al.

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Maria Eugenia Costa Queiroz et al.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2019)

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Liquid - Phase microextraction and electromembrane extraction in millifluidic devices: A tutorial

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ANALYTICA CHIMICA ACTA (2019)

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Fully Automated Electric-Field-Driven Liquid Phase Microextraction System with Renewable Organic Membrane As a Front End to High Performance Liquid Chromatography

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Miniaturized Matrix Solid-Phase Dispersion for the Analysis of Ultraviolet Filters and Other Cosmetic Ingredients in Personal Care Products

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Milos Dvorak et al.

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A New Microchip Design. A Versatile Combination of Electromembrane Extraction and Liquid-Phase Microextraction in a Single Chip Device

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Carbon nanotube-polymer composite for effervescent pipette tip solid phase microextraction of alkaloids and flavonoids from Epimedii herba in biological samples

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Mukul Sonker et al.

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Yulei Wang et al.

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Programmable flow-based dynamic sorptive microextraction exploiting an octadecyl chemically modified rotating disk extraction system for the determination of acidic drugs in urine

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Article Biochemical Research Methods

Efficient analysis of selected estrogens using fabric phase sorptive extraction and high performance liquid chromatography-fluorescence detection

Rajesh Kumar et al.

JOURNAL OF CHROMATOGRAPHY A (2014)

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Micro-electromembrane extraction across free liquid membranes. Extractions of basic drugs from undiluted biological samples

Pavel Kuban et al.

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Design and implementation of an automated liquid-phase microextraction-chip system coupled on-line with high performance liquid chromatography

Bin Li et al.

TALANTA (2014)

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Stir bar sorptive extraction: Recent applications, limitations and future trends

F. J. Camino-Sanchez et al.

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Review Chemistry, Analytical

On-chip microsolid-phase extraction in a disposable sorbent format using mesofluidic platforms

Manuel Miro

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2014)

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Nano-electromembrane extraction

Mara D. Ramos Payan et al.

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Magnetic nanoparticle assisted dispersive liquid-liquid microextraction for the determination of 4-n-nonylphenol in water

Kheng Soo Tay et al.

ANALYTICAL METHODS (2013)

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Chip-based liquid phase microextraction combined with electrothermal vaporization-inductively coupled plasma mass spectrometry for trace metal determination in cell samples

Han Wang et al.

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Stir bar sorptive extraction combined with high performance liquid chromatography-ultraviolet/inductively coupled plasma mass spectrometry for analysis of thyroxine in urine samples

Wenying Fan et al.

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The 12 principles of green analytical chemistry and the SIGNIFICANCE mnemonic of green analytical practices

Agnieszka Galuszka et al.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2013)

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Article Biochemical Research Methods

Parallel artificial liquid membrane extraction: micro-scale liquid-liquid-liquid extraction in the 96-well format

Astrid Gjelstad et al.

BIOANALYSIS (2013)

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Air-assisted liquid-liquid microextraction method as a novel microextraction technique; Application in extraction and preconcentration of phthalate esters in aqueous sample followed by gas chromatography-flame ionization detection

Mir Ali Farajzadeh et al.

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On-Chip Electro Membrane Extraction with Online Ultraviolet and Mass Spectrometric Detection

Nickolaj Jacob Petersen et al.

ANALYTICAL CHEMISTRY (2011)

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Matrix-assisted laser desorption/ionization mass spectrometry for quantitative determination of beta-blocker drugs in one-drop of human serum sample

Kamlesh Shrivas et al.

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Novel extraction approach for liquid samples: Stir cake sorptive extraction using monolith

Xiaojia Huang et al.

JOURNAL OF SEPARATION SCIENCE (2011)

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Quantitative determination of nicotinic acid in micro liter volume of urine sample by drop-to-drop solvent microextraction coupled to matrix assisted laser desorption/ionization mass spectrometry

Kamlesh Shrivas et al.

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Review Chemistry, Analytical

Solventless and solvent-minimized sample preparation techniques for determining currently used pesticides in water samples: A review

Maciej Tankiewicz et al.

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Implementation of droplet-membrane-droplet liquid-phase microextraction under stagnant conditions for lab-on-a-chip applications

Tiina Sikanen et al.

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New Automated and High-Throughput Quantitative Analysis of Urinary Ketones by Multifiber Exchange-Solid Phase Microextraction Coupled to Fast Gas Chromatography/Negative Chemical-Electron Ionization/Mass Spectrometry

Marco Pacenti et al.

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Adsorptive micro-extraction techniques-Novel analytical tools for trace levels of polar solutes in aqueous media

N. R. Neng et al.

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Stir rod sorptive extraction with monolithic polymer as coating and its application to the analysis of fluoroquinolones in honey sample

Yan-Bo Luo et al.

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Article Biochemical Research Methods

Low-density extraction solvent-based solvent terminated dispersive liquid-liquid microextraction combined with gas chromatography-tandem mass spectrometry for the determination of carbamate pesticides in water samples

Hao Chen et al.

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Development of a stir bar sorptive extraction based HPLC-FLD method for the quantification of serotonin reuptake inhibitors in plasma, urine and brain tissue samples

Nora Unceta et al.

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On-chip electro membrane extraction

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MICROFLUIDICS AND NANOFLUIDICS (2010)

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Stir Membrane Extraction: A Useful Approach for Liquid Sample Pretreatment

M. C. Alcudia-Leon et al.

ANALYTICAL CHEMISTRY (2009)

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Rotating-disk sorptive extraction of nonylphenol from water samples

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Determination of Polycyclic Aromatic Hydrocarbons in Drinking Water Samples by Solid-Phase Nanoextraction and High-Performance Liquid Chromatography

Huiyong Wang et al.

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A new liquid-phase microextraction method based on solidification of floating organic drop

Mohammad Reza Khalih Zanjani et al.

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Determination of organic compounds in water using dispersive liquid-liquid microextraction

Mohammad Rezaee et al.

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Directly suspended droplet microextraction

Lu Yangcheng et al.

ANALYTICA CHIMICA ACTA (2006)

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Electrokinetic migration across artificial liquid membranes - New concept for rapid sample preparation of biological fluids

S Pedersen-Bjergaard et al.

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Combining drop-to-drop solvent microextraction with gas chromatography/mass spectrometry using electronic ionization and self-ion/molecule reaction method to determine methoxyacetophenone isomers in one drop of water

HF Wu et al.

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Application of a novel ultra-low elution volume 96-well solid-phase extraction method to the LC/MS/MS determination of simvastatin and simvastatin acid in human plasma

AY Yang et al.

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Microextraction in packed syringe/liquid chromatography/electrospray tandem mass spectrometry for quantification of olomoucine in human plasma samples

M Abdel-Rehim et al.

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Single-drop microextraction combined with low-temperature electrothermal vaporization ICPMS for the determination of trace Be, Co, Pd, and Cd in biological samples

LB Xia et al.

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Thin-film microextraction

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ANALYTICAL CHEMISTRY (2003)

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Continuous-flow microextraction exceeding1000-fold concentration of dilute analytes

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