期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 88, 期 11, 页码 7525-7534出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.3c00370
关键词
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We present a general and efficient transition-metal-free C-C bond cross-coupling reaction of (hetero)-aryl ethers and diarylmethanes via C-(sp(2))-O bond cleavage. The coupling reactions mediated by KHMDS demonstrated high efficiency, broad substrate scope, and good functional group tolerance. The robustness and practicality of this protocol were further demonstrated by gram-scale preparation and diversified product derivatization.
We describe a general and efficient transition-metalfree C-Cbond cross-coupling of (hetero)-aryl ethers and diarylmethanes viaC-(sp(2))-O bond cleavage. The coupling reactions mediatedby KHMDS proceeded well with high efficiency, broad substrate scope,and good functional group tolerance. The robustness and practicabilityof this protocol also have been demonstrated by easy gram-scale preparationand diversified product derivatization.
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