Comparison of properties and application of starch nanoparticles optimized prepared from different crystalline starches

Starch nanoparticles (SNPs) were produced by nanoprecipitation combined with ultrasonication with the use of different starches (corn, potato and sago starch) and used to stabilize Pickering emulsions. The orthogonal experiment was used to optimize preparation conditions of gelatinization pretreatment duration of 30 min, ul-trasonic power of 600 W, and ultrasonic time of 40 min. Compared with native starch, the SNPs were spherical in shape and displayed a V-type crystalline structure with low relative crystallinity and higher degree of double -helix. Compared with native starch-Pickering emulsion, the SNP-Pickering emulsion had a smaller droplet size, more uniform distribution, clearer oil/water interface, and higher static stability of droplets. The sago SNP -Pickering emulsion had the great gelatinous structure and emulsion stability. In addition, the SNP-Pickering emulsion had the better loading efficiency and controlled release performance of curcumin. Meanwhile, the bioavailability of curcumin in sago SNP-Pickering emulsion was highest.

Automated summary

Starch nanoparticles were prepared by nanoprecipitation combined with ultrasonication and used to stabilize Pickering emulsions. The optimized preparation conditions resulted in spherical nanoparticles with low crystallinity and high double-helix structure, which improved the droplet size, distribution, and stability of the emulsion. Furthermore, the starch nanoparticle-Pickering emulsion exhibited enhanced loading efficiency and controlled release performance of curcumin.