期刊
JOURNAL OF THE ELECTROCHEMICAL SOCIETY
卷 163, 期 14, 页码 F1523-F1526出版社
ELECTROCHEMICAL SOC INC
DOI: 10.1149/2.0741614jes
关键词
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资金
- Research and Development Program of the Korea Institute of Energy Research (KIER) [B6-2442]
In this study, a novel electrolysis cell based on ethylenediamine (EDA) as a cathodic solvent was developed for NH3 electro-synthesis. The NH3-generating cathode chamber was filled with 0.1 M LiCl/EDA and separated by a cation exchange membrane from the anodic compartment, which was filled with 0.05 M H2SO4 aqueous solution. It appeared that EDA was cathodically stable, and thus electron-stealing medium destruction was substantially avoided. The faradaic efficiency for NH3 synthesis was 17.2%, producing 7.73 x 10(-7) mol NH3 for 1 h electrolysis at a cell voltage of 1.8 V with the charge consumption of 1.3 C. (C) 2016 The Electrochemical Society. All rights reserved.
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